scholarly journals Synthesis and Investigation of Antimicrobial Activity of Cu2O Nanoparticles/Zeolite

2017 ◽  
Vol 2017 ◽  
pp. 1-6 ◽  
Author(s):  
Bui Duy Du ◽  
Dang Van Phu ◽  
Le Anh Quoc ◽  
Nguyen Quoc Hien
Keyword(s):  
Electron Microscopy ◽  
Cuprous Oxide ◽  
Large Scale ◽  
Copper Ions ◽  
Zeolite A ◽  
X Ray Diffraction ◽  
X Ray ◽  
Agricultural Application ◽  
Transmission Electron ◽  
Cu2o Nanoparticles

Cuprous oxide (Cu2O) nanoparticles in zeolite A were synthesized by two steps: (i) ion-exchange of copper ions into the zeolite and (ii) reduction of copper ions in cages of the zeolite by hydrazine hydrate in base medium. The Cu2O nanoparticles/zeolite product was characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), and energy-dispersive X-ray spectroscopy (EDX). The particle size of Cu2O nanoparticles was of 40 nm. The antibacterial activity of the as-synthesized Cu2O nanoparticles/zeolite against Escherichia coli was also investigated. Cu2O NPs/zeolite product can be favorably produced on large scale for water treatment and agricultural application as antimicrobial agent.

Uniform Cerium-Based Coordination Polymer Microspheres: Preparation and Upconversion Emission

2016 ◽  
Vol 16 (4) ◽  
pp. 3705-3709 ◽  
Author(s):  
Zhi-Wen Nie ◽  
Cheng-Hui Zeng ◽  
Gang Xie ◽  
Sheng-Liang Zhong
Keyword(s):  
Electron Microscopy ◽  
Coordination Polymer ◽  
Large Scale ◽  
Upconversion Emission ◽  
X Ray Diffraction ◽  
X Ray ◽  
Band Emission ◽  
Transmission Electron ◽  
Light Excitation ◽  
Luminescent Spectra

Homogeneously doped Yb3+ and Er3+ cerium-based coordination polymer (CP) microspheres have been successfully synthesized on a large scale through a simple solvothermal route with 2, 5-pyridinedicarboxylic acid (2, 5-H2PDC) as the organic linker. CeO2:Yb3+, Er3+ porous microspheres were obtained by annealing the corresponding CP microspheres at 600 °C for 4 h under atmospheric pressure. These as-prepared products were characterized by Powder X-ray diffraction (PXRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FTIR), energy-dispersion X-ray (EDX) spectroscopy, Thermogravimetric (TG) and derivative thermogravimetric (DTG) analysis. The room temperature upconversion luminescent spectra of the as-prepared microspheres were carried out by 980 nm NIR light excitation. Interestingly, Yb3+ and Er3+ codoped CP microspheres give a single-band emission centered at 673 nm, while the CeO2:Yb3+, Er3+ microspheres give emission in green and red region, with red being the dominant emission. The emission intensity of the CeO2:Yb3+, Er3+ microspheres were much stronger than that of the Yb3+ and Er3+ codoped CP microspheres.

SYNTHESIS OF In2O3 NANOWIRES ENHANCED BY ANODIC ALUMINA MEMBRANE

2006 ◽  
Vol 05 (04n05) ◽  
pp. 479-485
Author(s):  
C. W. LAI ◽  
X. Y. ZHANG ◽  
H. C. ONG ◽  
J. Y. DAI ◽  
H. L. W. CHAN
Keyword(s):  
Electron Microscopy ◽  
Large Scale ◽  
Anodic Alumina ◽  
X Ray Diffraction ◽  
Alumina Membrane ◽  
Thermal Evaporation Method ◽  
Single Crystalline ◽  
X Ray ◽  
Alumina Membranes ◽  
Transmission Electron

Large-scale single crystalline In 2 O 3 nanowires were successfully synthesized on anodic alumina membranes by a simple thermal evaporation method at 570°C. X-ray diffraction, transmission electron microscopy, and scanning electron microscopy studies revealed the formation of single crystalline In 2 O 3 nanowires with diameters of 50–100 nm and lengths of up to a few hundreds of micrometers. Cathodeluminescence study revealed existence of oxygen vacancies evidenced by a strong and broad emission at 470 nm with a shoulder at 400 nm. The growth mechanism of the nanostructures is also discussed.

Characterization of Amorphized Zeolite A by Combining High-Energy X-ray Diffraction and High-Resolution Transmission Electron Microscopy

2012 ◽  
Vol 116 (48) ◽  
pp. 25293-25299 ◽  
Author(s):  
Kaku Sato ◽  
Toru Wakihara ◽  
Shinji Kohara ◽  
Koji Ohara ◽  
Junichi Tatami ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
High Resolution ◽  
High Energy ◽  
Zeolite A ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron

Mixed-Solvothermal Preparation of Mace-Like CdS Nanocrystals

2012 ◽  
Vol 502 ◽  
pp. 164-168
Author(s):  
Ling Xu ◽  
Han Mei Hu ◽  
Hai Yan Xu
Keyword(s):  
Electron Microscopy ◽  
Large Scale ◽  
Volume Ratio ◽  
X Ray Diffraction ◽  
Visible Absorption ◽  
X Ray ◽  
Transmission Electron ◽  
Cds Nanostructures ◽  
Uv Visible ◽  
Solvothermal Preparation

Novel mace-like (wolf-teeth clubs) CdS nanostructures were successfully prepared on a large scale using CdCl2•2.5H2O and NH2CSNH2 as starting materials through a convenient mixed-solvothermal route. The as-synthesized products were characterized by X-ray diffraction (XRD), energy dispersive X-ray spectrometry (EDX), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM) and UV-visible absorption spectroscopy. The experimental results reveal that the morphology of CdS products was greatly affected by the volume ratio of anhydrous ethanol and distilled water. The possible mechanism for the formation of mace-like CdS nanostructures is simply discussed.

scholarly journals Facile Synthesis of Calcium Carbonate Nanoparticles from Cockle Shells

2012 ◽  
Vol 2012 ◽  
pp. 1-5 ◽  
Author(s):  
Kh. Nurul Islam ◽  
A. B. Z. Zuki ◽  
M. E. Ali ◽  
Mohd Zobir Bin Hussein ◽  
M. M. Noordin ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Calcium Carbonate ◽  
Large Scale ◽  
Low Cost ◽  
Analytical Techniques ◽  
Variable Pressure ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Ft Ir

A simple and low-cost method for the synthesis of calcium carbonate nanoparticles from cockle shells was described. Polymorphically, the synthesized nanoparticles were aragonites which are biocompatible and thus frequently used in the repair of fractured bone and development of advanced drug delivery systems, tissue scaffolds and anticarcinogenic drugs. The rod-shaped and pure aragonite particles of30±5 nm in diameter were reproducibly synthesized when micron-sized cockle shells powders were mechanically stirred for 90 min at room temperature in presence of a nontoxic and nonhazardous biomineralization catalyst, dodecyl dimethyl betaine (BS-12). The findings were verified using a combination of analytical techniques such as variable pressure scanning electron microscopy (VPSEM), transmission electron microscopy (TEM), Fourier transmission infrared spectroscopy (FT-IR), X-ray diffraction spectroscopy (XRD), and energy dispersive X-ray analyser (EDX). The reproducibility and low cost of the method suggested that it could be used in industry for the large scale synthesis of aragonite nanoparticles from cockle shells, a low cost and easily available natural resource.

Electrochemical Fabrication of BixTe1-x (0.4 ≤ x ≤ 0.7) Nanowire Arrays

2007 ◽  
Vol 546-549 ◽  
pp. 2171-2174
Author(s):  
Wei Wang ◽  
J.F. Qu ◽  
X.L. Lu ◽  
G.Q. Zhang ◽  
Guang Li ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Large Scale ◽  
Atomic Ratio ◽  
Nanowire Arrays ◽  
X Ray Diffraction ◽  
Alumina Membrane ◽  
X Ray ◽  
Selected Area Electron Diffraction ◽  
Transmission Electron ◽  
Electrochemical Fabrication

Large scale and highly ordered thermoelectric BixTe1-x (0.4 ≤ x ≤ 0.7) nanowire arrays were successfully fabricated by cathodic electrolysis into porous anodic alumina membrane (AAM) templates in aqueous solution. The structure of the nanowires was characterized by X-ray diffraction and selected-area electron diffraction (SAED). Field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM) results show that the nanowires are smooth and uniform with the diameters of about 50 nm and lengths up to tens of micrometers. Energy dispersive spectroscopy (EDS) was used to check the exact stoichiometry of as-prepared samples. The results reveal that the atomic ratio between Bi and Te can be modulated effectively by controlling the concentration of the electrolyte solution. The synthesis of high quality BixTe1-x nanowires with controllable x is significant for optimizing the thermoelectric performance.

Epitaxial stabilization of orthorhombic cuprous oxide films on MgO(110)

2001 ◽  
Vol 16 (4) ◽  
pp. 914-921 ◽  
Author(s):  
Paul R. Markworth ◽  
R. P. H. Chang ◽  
Y. Sun ◽  
G. K. Wong ◽  
J. B. Ketterson
Keyword(s):  
Crystal Structure ◽  
Electron Microscopy ◽  
Cuprous Oxide ◽  
Equilibrium Phase ◽  
Metal Films ◽  
Epitaxial Films ◽  
X Ray Diffraction ◽  
Cubic Crystal ◽  
X Ray ◽  
Transmission Electron

Continuous epitaxial films of cuprous oxide (Cu2O) have been formed by the thermal oxidation of 1.5-μm-thick Cu metal films deposited on MgO(110) substrates. These films melted at 1118 °C in air, in agreement with equilibrium phase diagrams. Upon cooling from the liquid, a highly crystalline, epitaxial, 2.5-μm-thick Cu2O film was formed. X-ray diffraction spectroscopy revealed that the Cu2O film crystal structure was orthorhombically distorted from the bulk cubic crystal structure. High-resolution transmission electron microscopy showed that the film is coherent, and energy dispersive x-ray spectroscopy showed that interdiffusion is limited to the interface. These results suggest that a new epitaxially stabilized phase of Cu2O has been formed.

A High Resolution Study of G.P. Zones in Aluminum - 4.2 at % Silver

1982 ◽  
Vol 40 ◽  
pp. 722-723 ◽  
Author(s):  
R. Gronsky
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
High Resolution ◽  
Computer Simulations ◽  
Structural Characteristics ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Resolution Study

The phenomenon of clustering in Al-Ag alloys has been extensively studied since the early work of Guinierl, wherein the pre-precipitation state was characterized as an assembly of spherical, ordered, silver-rich G.P. zones. Subsequent x-ray and TEM investigations yielded results in general agreement with this model. However, serious discrepancies were later revealed by the detailed x-ray diffraction - based computer simulations of Gragg and Cohen, i.e., the silver-rich clusters were instead octahedral in shape and fully disordered, atleast below 170°C. The object of the present investigation is to examine directly the structural characteristics of G.P. zones in Al-Ag by high resolution transmission electron microscopy.

Identification of calcium oxalate crystals in dried or fixed tobacco leaf

1984 ◽  
Vol 42 ◽  
pp. 288-289
Author(s):  
Vicki L. Baliga ◽  
Mary Ellen Counts
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Calcium Oxalate ◽  
Growth And Development ◽  
Polarized Light ◽  
Calcium Oxalate Crystals ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Scanning Electron

Calcium is an important element in the growth and development of plants and one form of calcium is calcium oxalate. Calcium oxalate has been found in leaf seed, stem material plant tissue culture, fungi and lichen using one or more of the following methods—polarized light microscopy (PLM), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and x-ray diffraction.Two methods are presented here for qualitatively estimating calcium oxalate in dried or fixed tobacco (Nicotiana) leaf from different stalk positions using PLM. SEM, coupled with energy dispersive x-ray spectrometry (EDS), and powder x-ray diffraction were used to verify that the crystals observed in the dried leaf with PLM were calcium oxalate.

The Effect of the Microstructure of Diffusion Barriers on the Palladium Activation for Electroless Copper Deposition

2002 ◽  
Vol 716 ◽  
Author(s):  
Seok Woo Hong ◽  
Yong Sun Lee ◽  
Ki-Chul Park ◽  
Jong-Wan Park
Keyword(s):  
Electron Microscopy ◽  
Diffusion Barriers ◽  
Copper Deposition ◽  
X Ray Diffraction ◽  
Plan View ◽  
X Ray ◽  
Transmission Electron ◽  
Electroless Copper ◽  
Sheet Resistance Measurement ◽  
Scanning Electron

AbstractThe effect of microstructure of dc magnetron sputtered TiN and TaN diffusion barriers on the palladium activation for autocatalytic electroless copper deposition has been investigated by using X-ray diffraction, sheet resistance measurement, field emission scanning electron microscopy (FE-SEM) and plan view transmission electron microscopy (TEM). The density of palladium nuclei on TaN diffusion barrier increases as the grain size of TaN films decreases, which was caused by increasing nitrogen content in TaN films. Plan view TEM results of TiN and TaN diffusiton barriers showed that palladium nuclei formed mainly on the grain boundaries of the diffusion barriers.

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