scholarly journals ISOLASI DAN IDENTIFIKASI KOMPONEN KIMIA MINYAK ASIRI DAGING BUAH DAN FULI BERDASARKAN UMUR BUAH PALA (MYRISTICA FRAGRANS HOUTT)

2020 ◽  
Vol 20 (1) ◽  
pp. 69
Author(s):  
Angreni B. Liunokas ◽  
Ferry F. Karwur
Keyword(s):  
Information Source ◽  
Oil Quality ◽  
Economic Value ◽  
Chemical Components ◽  
Fourth Stage ◽  
Isolation And Identification ◽  
Myristica Fragrans ◽  
Third Stage ◽  
Myristica Fragrans Houtt

Abstrak: Pala (Myristica fragrans Houtt) sebagai bioreaktor hayati menghasilkan produk utama minyak asiri bernilai ekonomi tinggi yang tersebar pada bagian-bagian buahnya. Minyak asiri pala tersusun oleh kelompok besar terpenoid dan fenilpropanoid yang memiliki konsentrasi terkecil namun sebagai indikator mutu minyak pala. Penelitian tentang isolasi dan identifikasi komponen kimia minyak asiri daging buah dan fuli pala, telah dilaksanakan di Laboratorium CARC UKSW Salatiga dan Laboratorium Terpadu UII Yogyakarta. Penelitian ini bertujuan untuk mengetahui komponen kimia minyak asiri daging buah dan fuli pala berdasarkan tahapan perkembangan buah dan isolasi miristisin sebagai indikator dari kualitas minyak pala. Minyak asiri diperoleh dengan metode ekstraksi kemudian di analisis komponennya menggunakan Kromatografi Gas Spektrometri Massa (GC-MS). Hasil penelitian menunjukkan bahwa komponen kimia terbesar dari minyak asiri daging buah pala secara berturut-turut yaitu tahap pertama miristisin 36.05% pada retensi 11.57 menit, tahap kedua dan keempat α-pinen 39.16%; 34.64% retensi 3.53 menit, tahap ketiga sabinen 33.88% pada retensi 3.99 menit. Sedangkan pada minyak fuli tahap pertama hingga keempat yaitu sabinen 38.72%; 37.51%; 36.24%; 28.93% pada waktu retensi 3.99. Berdasarkan analisis GC-MS menunjukkan bahwa komponen senyawa yang dominan pada daging buah dan fuli yaitu miristisin, sabinen, α-pinen, β-pinen yang berkontribusi bagi aroma khas pada pala. Hasil penelitian diharapkan dapat dimanfaatkan sebagai sumber informasi penting dalam menghasilkan minyak asiri dengan kualitas baik dengan kandungan miristisin terbanyak.Kata Kunci : M. fragrans Houtt; isolasi; daging buah, fuli, minyak asiriAbstract: Nutmeg (Myristica fragrans Houtt) as a natural bioreactor produces the main product that is aetheric oil with a high economic value which is scattered on the parts of the fruit. Aetheric oil consists of a big group of terpenoid and phenylpropanoid which has the smallest concentration but functions as the indicator of nutmeg oil quality. The research about isolation and identification of chemical components of aetheric oil of pulp and mace has been conducted in CARC Laboratory of UKSW Salatiga and Integrated Laboratory of UII Yogyakarta. This current research aims at knowing the components of aetheric oil of nutmeg pulp and mace based on the development stages of the fruit and myristicin isolation as the indicator of the quality of nutmeg oil. Aetheric oil is formed by the extraction method. Then the components are analyzed by using Mass Spectrometry Gass Chromatography (GC-MS). The result of the research shows that respectively the biggest chemical component of aetheric oil consists of the first stage myristicin 36.05% on retention 11.57 minutes, second stage and fourth stage α-pinene 39.16%; 34.64% on retention 3.53 minutes, the third stage sabinene 33.88% on retention 3.99 minutes. Meanwhile on the mace oil, the first to the fourth stage is sabinene 38.72%; 37.51%; 36.24%; 28.93% on retention 3.99. Based on the analysis of GC-MS, it is shown that the most dominant compound components of pulp and mace are myristicin, sabinene, α-pinene, and β-pinene which contribute to the typical scent of nutmeg. The result of the research is expected to be used as an important information source in resulting in aetheric oil with good quality with the most myristicin content.Keywords: Myristica fragrans Houtt; isolation; pulp, mace, aetheric oil

scholarly journals Isolation and Identification of Essential Oil Made From Kisar Sweet Orange Peels

2021 ◽  
Vol 1 (1) ◽  
pp. 1-11
Author(s):  
Gelora Helena Augustyn ◽  
Anthonia Matjora ◽  
Vita N Lawalata ◽  
Sophia G Sipahelut
Keyword(s):  
Essential Oil ◽  
Steam Distillation ◽  
Sweet Orange ◽  
Economic Value ◽  
Acid Number ◽  
Chemical Components ◽  
Distillation Method ◽  
Isolation And Identification ◽  
Orange Peels

Kisar sweet orange is an endemic fruit and primary commodity from Kisar Island, Southwest Maluku Regency - Maluku Province. Currently, Kisar sweet orangeswere only consumed as fresh fruit during this time, partially processed into juice and the peels were discarded as wastes. Kisar sweet orange peels can be processed into essential oil to increase their economic value. The essential oil made from orange peels is highly preferable, especially for the middle to upper-class consumers, for health and air-freshening purposes.  This essential oil has a higher selling value. This research aims at isolating and identifying the chemical components and quality of essential oil made from Kisar sweet orange peels. This essential oil was isolated using a steam distillation method, and its chemical components were identified using GC-MS instruments.. The research results showed that the essential oil made from Kisar sweet orange peels dried with a cabinet dryer for two days utilizing the steam distillation method provides a yield of 0.53%, with its properties of specific gravity of 0.8457, refractive index of 1.4651 (20°C), acid number of 1.92, ester number of 8.05, and solubility in alcohol of 1:9. The main chemical component of the essential oil made from Kisar sweet orange peels detected by GC-MS is limonene (70.80%).

scholarly journals EKSPLORASI DAN IDENTIFIKASI CENDAWAN ANTAGONIS TERHADAP JAMUR AKAR PUTIH (Rigidoporus lignosus) PADA TANAMAN PALA (Myristica fragrans Houtt)

2020 ◽  
Vol 4 (2) ◽  
Author(s):  
Nana Ariska ◽  
Lola Adres Yanti ◽  
Chairudin Chairudin
Keyword(s):  
Economic Value ◽  
Culture Method ◽  
Dilution Method ◽  
Dual Culture ◽  
Trichoderma Spp ◽  
Pests And Diseases ◽  
Myristica Fragrans ◽  
Rigidoporus Lignosus ◽  
Myristica Fragrans Houtt

Nutmeg (Myristica fragrans Houtt) is a multipurpose plantation commodity crop that almost all parts of the plant have strategic economic value to be cultivated. In Indonesia there are the largest nutmeg commodity centers, including the Maluku islands, North Sulawesi and Aceh. The biggest problem with nutmeg plants is the attack of pests and diseases. One of the most severe diseases in nutmeg is white root mushroom (Rigidoporus lignosus). This study aims to 1) determine the fungus of white root fungus antagonists (Rigodoporus lignosus) from the Aceh nutmeg rhizosphere (Myristica fragrans Houtt), 2) identify the content of antibiotic fungus JAP antagonist compounds in Aceh nutmeg plants. The study was conducted by taking soil samples from nutmeg plants at three nutmeg plantations in South Aceh. The antagonist fungus isolation activity uses a dilution method. Isolation of JAP from infected roots using direct planting method. Furthermore, it is identified macroscopically and microscopically. The antagonist test was carried out using the dual culture method with RAL. From the rhizosphere in the nutmeg area, 5 candidate antagonist isolates were obtained, having high in vitro antagonism ability to the pathogen R. lignosus. Identification results showed that isolates 1, 2 and 3 were Trichoderma spp, and isolates 4 and 5 were Gliocladium virens. Keywords: In vitro, the content of antibiotic compounds, Aceh nutmeg, Rigidoporus lignosus, antagonistic test

scholarly journals Kinetic Degradation of Myristicin, Elemicin, and Safrole in Encapsulated Banda Nutmeg (Myristica fragrans Houtt) Oleoresin

2017 ◽  
Vol 14 (1) ◽  
pp. 43
Author(s):  
Dewi Amrih ◽  
Chusnul Hidayat ◽  
Pudji Hastuti
Keyword(s):  
Activation Energy ◽  
Physicochemical Properties ◽  
Spray Drying ◽  
Myristica Fragrans ◽  
Drying Techniques ◽  
Myristica Fragrans Houtt ◽  
Dark Glass ◽  
C 50 ◽  
Flavoring Agent

Spices, in the form of oleoresin, have advantages as a flavoring agent. Nutmeg oleoresin compounds that play an important role in the formation of nutmeg flavor are myristicin, elemicin, and safrole. These compounds are not stable, so that the quality of oleoresin decreased easily. An alternative to overcome this problem is the encapsulation of oleoresin using spray drying techniques. The objective of this research was to evaluate the physicochemical properties of oleoresin with respect to the degradation of myristicin, elemicin, and safrole of nutmeg oleoresin. Microencapsulated nutmeg oleoresin was prepared using 12% WPC and 88% maltodextrin as encapsulate materials. It was stored in dark glass bottles at a various temperature, namely 30°C, 40°C, 50°C, 60°C, and 70°C, for 0, 4, 7, 10, 14, 21, 28, 35, 42, 49, 56 and 63 days. The content of myristicin, elemicin, and safrole were analysed. The results showed that myristicin, elemicin, and safrole in the encapsulated nutmeg oleoresin decreased during the storage until 28 days of storage and then they were relatively stable until 63 days. The activation energy of myristicin, elemicin, and safrole were 2.21 kJ/mol.K, 2.71 kJ/mol.K and 3.22 kJ/mol.K, respectively.

scholarly journals Larvicidal Activity of Essential Oils from the Leaves and Fruits of Nutmeg (Myristica fragrans Houtt) Against Aedes aegypti (Diptera: Culicidae)

2016 ◽  
Vol 4 (7) ◽  
pp. 552
Author(s):  
Anne Carolina ◽  
Maman Maman
Keyword(s):  
Essential Oil ◽  
Aedes Aegypti ◽  
Larvicidal Activity ◽  
Steam Distillation ◽  
Chemical Compounds ◽  
Chemical Components ◽  
Myristica Fragrans ◽  
Leaf Oil ◽  
Myristica Fragrans Houtt ◽  
Fruit Oil

The aim of this research was to examine the larvicidal activity of essential oil (EO) extracted from nutmeg (Myristica fragrans Houtt) leaves and fruits by steam distillation, and to analyze its chemical compounds. The EO yield of nutmeg leaves and fruits collected from the same tree was 0.66% and 0.30%, respectively. Larvicidal tests with the EO were carried out against Aedes aegypti (L.) (Diptera: Culicidae). The concentrations of nutmeg EO used for the larvicidal assay were 50, 100, 150, 200, and 250 μg/mL. The results showed that fruit oil was more toxic than the leaf oil. LC50 values of leaf and fruit EOs were 133.8 and 110.1 µg/mL, respectively. The chromatogram of GC-MS showed that the chemical components in nutmeg leaf and fruit EOs were dominated by α-pinene, sabinene, β-pinene, delta-3-carene, limonene, β-phellandrene, α-terpinolene, linalool, safrole, croweacin, and myristicin.

scholarly journals Pengaruh Ukuran Bahan terhadap Rendemen dan Kualitas Minyak Biji Pala (Myristica Fragrans Houtt) dengan Metode Soxhletasi

Jurnal MIPA ◽  
2018 ◽  
Vol 7 (1) ◽  
pp. 39
Author(s):  
Andika Saranaung ◽  
Meiske S. Sangi ◽  
Dewa G. Katja
Keyword(s):  
Seed Oil ◽  
Acid Number ◽  
Peroxide Number ◽  
Value Set ◽  
Myristica Fragrans ◽  
Myristica Fragrans Houtt

Indonesia merupakan salah satu negara yang mempunyai berbagai jenis tanaman yang dapat dimanfaatkan oleh manusia, salah satunya ialah tanaman rempah-rempah. Di antara rempah-rempah utama Indonesia, pala merupakan salah satu rempah-rempah yang cukup tinggi nilainya sehingga perlu dikembangkan pemanfaatannya. Tujuannya menentukan rendemen dan kualitas minyak biji pala 60 mesh, 40 mesh, dan 20 mesh yang diambil dari kabupaten kepulauan talaud dengan metode soxhletasi. Metode yang digunakan adalah soxhletasi dengan pelarut n-hexan. Kualitas minyak biji pala diperoleh dengan menguji bilangan asam, bilangan peroksida, bilangan ester, dan kelarutan dalam etanol 90%. Hasil yang diperoleh dengan soxhletasi minyak biji pala rendemennya adalah 60 mesh (39,61%), 40 mesh (37,52%), dan 20 mesh (28,09%). Bilangan asam 60 mesh (3,9777%), 40 mesh (3,8967%), dan 20 mesh (3,4928%). Bilangan peroksida 60 mesh (0,0114%), 40 mesh (0,0118%), dan 20 mesh (0,0149%). Bilangan ester 60 mesh (29,2059%), 40 mesh (30,0777%), dan 20 mesh (31,5288%), dan kelarutan dalam etanol 90% mendekati nilai yang ditetapkan SNI yaitu 1:1. Hasilnya menunjukkan bahwa rendemen minyak biji pala paling banyak adalah 60 mesh dan kualitas minyak terbaik adalah 20 mesh.Indonesia is a country which has various types of plants that can be utilized by humans one of plants is a spice plant. Among the main spices of Indonesia, nutmeg is one of the spices that is high enough value so that it needs to be developed utilization. The purpose of this research is to determine the rendemen and  its quality of nutmeg seed oil of 60 mesh, 40 mesh, and 20 mesh taken from talaud islands by soxhletasi method with n-hexan solvent. The quality of nutmeg seed oil obtained by testing acid number, peroxide number, ester number, and solubility in ethanol 90%. The results obtained with soxhletasi of nutmeg seed oil are 60 mesh (39,61%), 40 mesh (37,52%), and 20 mesh (28,09%). Acid numbers are 60 mesh (3,9777%), 40 mesh (3,8967%), and 20 mesh (3,4928%). Peroxide numbers are 60 mesh (0,0114%), 40 mesh (0,0118%), and 20 mesh (0,0149%). The ester numbers are 60 mesh (29,2059%), 40 mesh (30,0777%), and 20 mesh (31,5288%), and the solubility in ethanol is 90% close to the value set by the SNI that is 1:1. The results show that the rendement of 60 mesh nutmeg seed oil is most and the best quality oil is 20 mesh

scholarly journals Physico-chemical Properties of Nutmeg (Myristica fragrans houtt) of North Sulawesi Nutmeg

2020 ◽  
Vol 5 (1) ◽  
pp. 23
Author(s):  
Dino Rahardiyan ◽  
Mario Poluakan ◽  
Emma Mauren Moko
Keyword(s):  
Optical Rotation ◽  
Economic Value ◽  
Chemical Properties ◽  
Full Potential ◽  
North Sulawesi ◽  
Myristica Fragrans ◽  
Oil Extract ◽  
Optical Rotations ◽  
Myristica Fragrans Houtt ◽  
The Many

Essential oil of nutmeg (Myristica fragrans houtt) is one of the many potentials of nutmeg that has a high economic value although in North Sulawesi it has not been exploited to its full potential. This research was conducted to compare the yield and properties of Nutmeg oil extract from the seeds and mace of Talaud and North Minahasa-North Sulawesi. The oil extract was obtained by distillation and was further characterized in terms of color, solubility in ethanol, density, optical rotation, refractive index.  Results of this research exhibited that oil of the mace of nutmeg from Talaud had a lighter appearance in color compared to that from North Minahasa, while the density of oil extracted from North Minahasa was more densed compared to Talaud in both seed and mace (0.923 and 0.938 respectively at 25°C). The reflective index of nutmeg oil from North Minahasa was slightly higher than of Talaud both from seed and mace (1.4834 and 1.493 at 25°C), while the optical rotations of oil extracted from the mace were between +6.90° to +9.80° and from the seed were +20.73° to +22.30°.

scholarly journals Isolation and Identification of Flavonoid Compound from Nutmeg Leaves (Myristica fragrans Houtt)

2016 ◽  
Vol 28 (1) ◽  
pp. 199-202 ◽  
Author(s):  
Binawati Ginting ◽  
Lamek Marpaung ◽  
Tonel Barus ◽  
Partomuan Simanjuntak
Keyword(s):  
Flavonoid Compound ◽  
Isolation And Identification ◽  
Myristica Fragrans ◽  
Myristica Fragrans Houtt

scholarly journals On-farm evaluation of seed yield and oil quality of linseed (Linum usitatissimum L.) in inland areas of Tuscany, Central Italy

2016 ◽  
Vol 11 (3) ◽  
pp. 199 ◽  
Author(s):  
Luciana G. Angelini ◽  
Silvia Tavarini ◽  
Daniele Antichi ◽  
Lara Foschi ◽  
Marco Mazzoncini
Keyword(s):  
Seed Yield ◽  
Linum Usitatissimum ◽  
Cropping Systems ◽  
Oil Quality ◽  
Economic Value ◽  
Central Italy ◽  
Weather Conditions ◽  
Oil Composition ◽  
Valuable Alternative

Traditional oilseed crops, such as linseed (<em>Linum usitatissimum</em> L.), may represent valuable alternative crops in cropping systems dominated by cereals, due to their adaptability to poor soils and to their high economic value related to the interesting quality of the oil, which is being increasingly appreciated by consumers and industry. The aim of this study was to test the adaptability of linseed to the inland marginal areas of Tuscany, and to explore the levels of crop yield and oil quality which can be achieved in hilly and lowland environments. For three years (2011-2014), experimental open fields (1- 5 ha each) were established and monitored in six commercial farms located in the inland countryside of Pisa province, Tuscany, Central Italy. The effect of environment (hilly and plain areas) was assessed in terms of yield and yield components as well as oil content and composition. Interestingly, seed yield and biomass production were very stable over years in the two areas of cultivation, irrespectively of yearly differences in weather conditions. As expected, higher yields were obtained in plain than in hilly areas. Regarding oil composition, oil extracted from linseed grown in plain environments was richer in linolenic acid, while, oppositely, both oleic and linoleic acids were more abundant in oil from hilly areas. Definitively, our results demonstrated that linseed might be a valuable alternative to cereal crops for marginal lands of Tuscany and, more in general, of Central Italy.

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