Study on Antistatic Modification of Carbon Nanotube on Silk Fabric

2013 ◽  
Vol 821-822 ◽  
pp. 51-54 ◽  
Author(s):  
Yu Chun Jiang ◽  
Li Man Chen ◽  
Xun Huang ◽  
Hua Ping Zeng ◽  
Jun Liang Zhang ◽  
...  
Keyword(s):  
Electrical Conductivity ◽  
Carbon Nanotube ◽  
Reaction Time ◽  
Reaction Temperature ◽  
Ph Value ◽  
Adsorption Property ◽  
Silk Fabric ◽  
Antistatic Property ◽  
New Type ◽  
Silk Fabrics

Carbon nanotube is a new type of nanoscale materials, which has excellent adsorption property and electrical conductivity. In this paper, silk fabrics were antistatic modified by adsorption of carbon nanotube. The results indicate that the optimum modified conditions are summed up as follows: quality ratio of carbon nanotube and silk fabric is 1:5, pH value is 4, reaction temperature is 95°C and reaction time is 1.5 h. The antistatic property of silk fabric which modified by carbon nanotube is obviously improved.

Experimental Research on Adsorption of Cadmium with Synthetic Tobermorite from Wastewater

2010 ◽  
Vol 160-162 ◽  
pp. 1038-1043 ◽  
Author(s):  
Hong Bin Qi ◽  
Hai Du ◽  
Cong Cong Yin
Keyword(s):  
Reaction Time ◽  
Reaction Temperature ◽  
Ph Value ◽  
Adsorption Property ◽  
Orthogonal Experiment ◽  
Research Work ◽  
Potassium Feldspar ◽  
Adsorption Efficiency ◽  
Isothermal Adsorption ◽  
Initial Concentration

Tobermorite nano-scale powder was synthesized from potassium feldspar ore from Henan province Lushi country in China. In the present research work, its adsorption property to Cd2+ was studied. The factors of adsorption such as pH values, traction time, initial concentration, and temperature were studied. The adsorption equation was curvefitted by the Langmuir and Freundlich adsorption isotherm and the thermodynamics adsorption was analyzed. By the orthogonal experiment and single-factor experiment of the adsorption, the optimized conditions of the adsorption for Cd2+ were achieved: the reaction temperature is 40°C, the reaction time is 20 min, the initial concentration of aqueous solution is 20 mg•L-1 and pH value is 6.0. Under these conditions the adsorption efficiency of Cd2+ can reach 99.89%. The orthogonal experimental results show that the order of effect on adsorption efficiency was the initial concentration, pH value, reaction temperature, reaction time. In different temperatures, the results show that isothermal Langmuir equation can describe the isothermal adsorption characteristics of Cd2+ on tobermorite. Thermodynamic parameters can be drawn: the G was negative and with increasing temperature H increased, so the adsorption process is a spontaneous reaction to the heat.

scholarly journals Facile Synthesis of Silver Nanoparticles and Preparation of Conductive Ink

Nanomaterials ◽  
2022 ◽  
Vol 12 (1) ◽  
pp. 171
Author(s):  
Gui Bing Hong ◽  
Yi Hua Luo ◽  
Kai Jen Chuang ◽  
Hsiu Yueh Cheng ◽  
Kai Chau Chang ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Electrical Resistivity ◽  
Reaction Time ◽  
Reaction Temperature ◽  
Ph Value ◽  
Chemical Reduction ◽  
Flexible Substrate ◽  
Synthesis Method ◽  
Future Research ◽  
Conductive Ink

In the scientific industry, sustainable nanotechnology has attracted great attention and has been successful in facilitating solutions to challenges presented in various fields. For the present work, silver nanoparticles (AgNPs) were prepared using a chemical reduction synthesis method. Then, a low-temperature sintering process was deployed to obtain an Ag-conductive ink preparation which could be applied to a flexible substrate. The size and shape of the AgNPs were characterized by ultraviolet–visible spectrophotometry (UV-Vis) and transmission electron microscopy (TEM). The experiments indicated that the size and agglomeration of the AgNPs could be well controlled by varying the reaction time, reaction temperature, and pH value. The rate of nanoparticle generation was the highest when the reaction temperature was 100 °C within the 40 min reaction time, achieving the most satisfactorily dispersed nanoparticles and nanoballs with an average size of 60.25 nm at a pH value of 8. Moreover, the electrical resistivity of the obtained Ag-conductive ink is controllable, under the optimal sintering temperature and time (85 °C for 5 min), leading to an optimal electrical resistivity of 9.9 × 10−6 Ω cm. The results obtained in this study, considering AgNPs and Ag-conductive ink, may also be extended to other metals in future research.

Enhanced Photocatalytic Performance and Mechanism of Ag3PO4 Particles Synthesized via a Sonochemical Process

2018 ◽  
Vol 10 (3) ◽  
pp. 337-345 ◽  
Author(s):  
Chengxiang Zheng ◽  
Hua Yang ◽  
Yang Yang ◽  
Haimin Zhang
Keyword(s):  
Particle Size ◽  
Photocatalytic Activity ◽  
Reaction Time ◽  
Reaction Temperature ◽  
Ph Value ◽  
Dye Degradation ◽  
Sonochemical Method ◽  
Simulated Sunlight ◽  
Spherical Nanoparticles ◽  
Direct Oxidation

A facile sonochemical method was used to synthesize Ag3PO4 particles and the effect of pH value, reaction temperature and reaction time on the products was investigated. It is found that the samples prepared at neutral (pH = 7) and alkaline (pH = 11) environments exhibit a similar particle morphology and size. The particles are shaped like spheres with a size distribution majorly focusing on a range of 200–450 nm, and the average particle size is about 300 nm. The sample prepared at acidic environment (pH = 3) is composed of polyhedral microparticles with size of 5–8 μm. At relatively low temperatures of 20–50 °C, the spherical nanoparticles do not undergo obvious morphology/size changes; however, when the temperature is increased up to 80 °C, the nanoparticles are aggregated to form large-sized polyhedral microparticles in the size range of 4–7 μm. Compared to the pH value and reaction temperature, the reaction time has a minor effect on the morphology of Ag3PO4 particles. RhB was chosen as the target pollutant to evaluate the photocatalytic activity of the as-prepared Ag3PO4 samples under simulated-sunlight irradiation. It is shown that the samples consisting of spherical nanoparticles exhibit an extremely high photocatalytic activity, and the degradation percentage of RhB after reaction for 50 min reaches over 90%. The samples of polyhedral microparticles have a relatively low photocatalytic activity, which is possibly due to their large particle size. Hydroxyl (.OH) radical was detected by spectrofluorimetry using terephthalic acid as a .OH scavenger and was not found to be produced over the simulated-sunlight-irradiated Ag3PO4 catalyst. The effect of ethanol, benzoquinone and ammonium oxalate on dye degradation was also investigated. Based on experimental results, the direct oxidation by h+ is suggested to the dominant mechanism toward the dye degradation.

Study on the Preparation of Chitosan-Based Resin

2010 ◽  
Vol 160-162 ◽  
pp. 1810-1815
Author(s):  
Jing Xian Li ◽  
Juan Qin Xue ◽  
Ming Wu ◽  
Yu Jie Wang ◽  
Wei Bo Mao
Keyword(s):  
Reaction Time ◽  
Reaction Temperature ◽  
Experimental Results ◽  
Raw Material ◽  
Cross Linking ◽  
Reactant Ratio ◽  
Experimental Conditions ◽  
Stirring Rate ◽  
Formaldehyde Crosslinking ◽  
New Type

With chitosan as the raw material, a new type of resin material is synthesized through formaldehyde crosslinking. The effects of the reactant ratio, the reaction temperature, the reaction time, the stirring rate and the system pH on the cross-linking rate are studied in detail. The resin material is then characterized by means of IR. The experimental results show that the reaction occurs mainly on the amino and the hydroxyl of chitosan. The chitosan-based resin material with good properties of sphericity and acidresistivity can be prepared under the optimal experimental conditions, which are found to be 1:5 for the ratio of chitosan and formaldehyde, 60°C for the temperature, 1 h for the reaction time, 440r/min for the stirring rate and 10 for the pH.

Preparation of Carboxymethylcellulose Picric Acid Ester and Adsorption Property for Creatinine

2010 ◽  
Vol 113-116 ◽  
pp. 1955-1958
Author(s):  
Xiao Feng Dai ◽  
Gui Zhen Fang
Keyword(s):  
Reaction Time ◽  
Reaction Temperature ◽  
Mass Fraction ◽  
Adsorption Property ◽  
Picric Acid ◽  
Reaction Conditions ◽  
Element Analysis ◽  
Monolayer Adsorption ◽  
Adsorption Amount ◽  
Isothermal Curve

Ether of carboxymethylcellulose-based picric acid(CMC-PA) was prepared from carboxymethylcellulose(CMC) and picric acid(PA) by the mild reactive conditions of acidylation with chloric.The strcture of CMC-PA was characterized by FTIR,Element analysis,XRD and CPMAS13C NMR.Influences of reaction conditions,such as reaction temperature,reaction time,ratio of CMC to PA and amount of pyridine,were studied by mass fraction of nitrogen.Result showed that the synthetical conditions were obtained as ratio of CMC to PA 2 : 1 (by weight),amount of pyridine 50 mL,reaction temperature 85°C and reaction time 4 hours.The adsorption property of CMC-PA to creatinine was studied under simulated biological human body conditons.The kinetic and isothermal curve were given. Results showed that adsorption amount reached an equilibrium value after 10 hours,and the maximum adsorption amount was 1.75mg/g.Equilibrium data of creatinine fit well with Freundich equation,indicating that the adsorption was mainly chemical monolayer adsorption .The Freundich indx(1/n) was less than 1,which implied that the adsorption was preferential process.

Study on Catalytic Degradation of Diesel Pollution in Seawater by Laccase

2013 ◽  
Vol 781-784 ◽  
pp. 2324-2327
Author(s):  
Xu Zheng ◽  
Xiao Cai Yu ◽  
Yun Qing Liu ◽  
Xiao Xv ◽  
Jin Fang Chen
Keyword(s):  
Reaction Time ◽  
Reaction Temperature ◽  
Sea Water ◽  
Oil Pollution ◽  
Ph Value ◽  
Degradation Process ◽  
Catalytic Degradation ◽  
Initial Concentration ◽  
Optimization Study ◽  
Optimum Reaction

Sea water joining diesel was selected to prepare simulated marine oil pollution. With the target of removing diesel from seawater, the influence of various factors on the laccase-catalyzed degradation process was discussed. The experimental results show that the laccase-catalyzed degradation process was significantly affected by laccase dosage, reaction temperature, reaction time, pH of the solution and initial concentration of diesel in the oily wastewater. A systematic optimization study was carried out through a orthogonal test on the basis of the results of the single-factor experiments,and the optimum reaction conditions of laccase catalytic degradation diesel pollutants in seawater was determined. The results indicate that under the conditions of diesel initial concentration of 0.1g/L, laccase dosage of 8mg/L, pH value of 6, the reaction temperature of 25°C and the reaction time of 4h, laccase catalytic degradation rate of diesel pollution can be up to 63.85%.

The Preparation Technique of Nanometer Molybdenum Trioxide by Hydrothermal Synthesis

2011 ◽  
Vol 117-119 ◽  
pp. 807-810
Author(s):  
Ji Wen Li ◽  
Yan Hua Ma ◽  
Fang Fang Gong ◽  
Guo Shang Zhang ◽  
Liu Jie Xu ◽  
...  
Keyword(s):  
Reaction Time ◽  
Hydrothermal Synthesis ◽  
Reaction Temperature ◽  
Molybdenum Trioxide ◽  
Ph Value ◽  
Ultrafine Particle ◽  
Preparation Technique ◽  
Optimum Ph ◽  
Optimum Reaction ◽  
Optimal Reaction

The technique of hydrothermal synthesis is used to prepare nanometer molybdenum trioxide through controlling the parameters such as the acidification condition, the reaction temperature, the reaction time and so on. The technique is under high temperature and high pressure by water as the solvent. Synthesized molybdenum trioxide powder is characterized by XRD, SEM, and HRTEM. The optimal reaction time is 40h, the optimum reaction temperature is 170°C, and the optimum pH value is 1.0. The results indicate that powder has an ultrafine particle size, high purity, and narrow size distribution, good fluidity, light agglomerate and is perfect in crystal.

Research on Preparation of Nano-Hydroxyapatite Biological Material

2013 ◽  
Vol 791-793 ◽  
pp. 303-306
Author(s):  
Yong Guang Bi ◽  
Xu Si Xu
Keyword(s):  
Particle Size ◽  
Reaction Time ◽  
Reaction Temperature ◽  
Ph Value ◽  
Spherical Shape ◽  
Temperature Reaction ◽  
Hydroxyapatite Nanoparticles ◽  
Uniform Size ◽  
Regular Shape ◽  
Particle Sample

In order to obtain hydroxyapatite nanoparticles smaller particle size distribution is relatively uniform, spherical shape and the particle sample, by exploring the reaction temperature, reaction time, concentration and pH on hydroxyapatite nanosize and distribution impact conditions, the results show that when the reaction temperature is 50°C; reaction time 2h; concentration 0.6mol/L; pH value of 10, the prepared nanohydroxyapatite regular shape, less agglomeration, uniform size high crystallinity. Description concentration and pH on nanoparticle size has a significant impact.

scholarly journals PENGARUH SUHU REAKSI, KECEPATAN PENGADUKAN DAN WAKTU REAKSI PADA PEMBUATAN SABUN PADAT DARI MINYAK KELAPA (Cocos nucifera L.)

2019 ◽  
Vol 8 (1) ◽  
pp. 11-17
Author(s):  
Rosdanelli Hasibuan ◽  
Fransiska Adventi ◽  
Rahmad Parsaulian Rtg
Keyword(s):  
Reaction Time ◽  
Moisture Content ◽  
Reaction Temperature ◽  
Ph Value ◽  
Cocos Nucifera ◽  
Coconut Oil ◽  
Operating Conditions ◽  
Animal Fats ◽  
Cocos Nucifera L ◽  
Impeller Type

Soap is a cleanser made by chemical reactions between sodium hydroxide or potassium hydroxide with fatty acids from vegetable oils or animal fats. Soaps can be made by several methods, namely saponification and neutralization methods, in this study carried out by saponification method. In the saponification method there are several problems namely operating conditions which include reaction temperature, stirring speed and stirring time. Therefore, need to do research to determine the best conditions of saponification reaction, namely reaction speed, operating temperature and reaction time using an impeller type multiple pitch blade turbine with research variables reaction temperature 60 oC, 70 oC, and 80 oC, stirring speed 300 rpm,400 rpm and 500 rpm and reaction time of 45minutes, 60 minutes, and 75 minutes. Saponification reaction is carried out by heating coconut oil and inserting 30% NaOH slowly and then stirring with a multiple pitch blade stirrer. The product will be analyzed by testing alkaline levels, moisture content and pH of the soap. The best operating conditions obtained from this study were at a temperature of 70 oC, reaction time of 60 minutes, stirring speed of 400 rpm with a pH value of 9.4 and an alkaline level of 0.073 and a moisture content of 9.8.

Study on Saccharification and Hydrolysis in Cellulose of Bagasse

2011 ◽  
Vol 236-238 ◽  
pp. 428-431
Author(s):  
Ying Xiao Mu ◽  
Hong Xiang Zhu ◽  
Hui He ◽  
Hai Nong Song ◽  
Shuang Fei Wang ◽  
...  
Keyword(s):  
Reaction Time ◽  
Reaction Temperature ◽  
Ph Value ◽  
Cellulose Hydrolysis ◽  
Reducing Sugar ◽  
Optimum Conditions ◽  
Value System ◽  
Percent Conversion ◽  
Substrate Size ◽  
Bagasse Pulp

The effect of the reaction time, the amount of enzyme, the reaction temperature and the pH value system, also the substrate size on bagasse pulp cellulose hydrolysis in the rate of reducing sugar was studied. And the optimum conditions response was researched. Under these conditions, we also studied the percent conversion of reducing sugar, and analyzed the changes of crystallinity after the bagasse pulp cellulose hydrolysis.

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