Mechanical characterization and creep strengthening of AZ91 magnesium alloy by addition of yttrium oxide nanoparticles

In the current research, the authors have attempted to improve the mechanical properties and creep behavior of the magnesium alloy Mg–9Al–1Zn (AZ91) in three different stress levels. To this end, the present study investigated experimentally the addition effects of different values of yttrium oxide nanoparticles to the AZ91. In this regard, weight percentages of 0.5%, 1%, 1.5%, and 2% nanoparticles were added to the material using the vortex casting method. Then, various test specimens were fabricated based on the ASTM standards by utilizing a Computer Numerical Control lathe machine. Different experiments were performed, and the results of different groups were compared with each other. The results revealed that the addition of yttrium oxide (Y2O3) nanoparticles increases the strength of AZ91 magnesium alloy until the nanoparticles do not clump in the microstructure. In other words, the tensile strength of the nanocomposite increased by adding nanoparticles up to 1.5%, but by adding 2% of nanoparticles, we found that the tensile strength is lower than that of pure magnesium. Moreover, one of the most important achievements of this study is that if the nanoparticles do not clump in the material microstructure, the addition of Y2O3 increases the rate of stable creep (the secondary creep stage). Also, the experimental results indicated that the highest stable creep rate is related to the nanocomposite with 1.5% yttrium oxide nanoparticles. Furthermore, the maximum hardness of the material was obtained in the same case.

Effects of temperature and load during hot impression behavior of Cr-Ni stainless steel

Austenitic Stainless steels are majorly used because of their high resistance to aqueous corrosion and high temperature properties. Some major applications of stainless steels at high temperatures include engine and exhaust components in aircrafts, recuperators in steel mills, and pulverized coal injection lances for blast furnaces. In all the above said applications, the components are constantly subjected to loads and high temperatures. This makes the study of their creep behavior very important to decide the life of the component. Cr-Ni stainless steel was used as a starting material, and hot impression creep test was performed on cylindrical samples of 10 mm height and 15 mm diameter for a dwell time of 150 min at two different loads of 84 and 98 MPa and at two different temperatures 450 and 500 °C. The time vs. indentation depth was plotted, and creep rate was calculated in each case. It was observed that with an increase in time, creep rate increased in the primary creep region and remained almost constant in the secondary creep region irrespective of temperature and load. The indentation depth and creep rate increased with an increase in load and temperature.

Nanoindentation Characterization of Creep-fatigue Interaction on Local Creep Behavior of P92 Steel Welded Joint

In modern fossil and nuclear power plants, the components are subjected to creep, fatigue, and creep-fatigue (CF) due to frequent start-up and shut-down operations at high temperatures. The CF interaction on the in-service P92 steel welded joint was investigated by strain-controlled CF tests with different dwell times of 30, 120, 300, 600 and 900 s at 650 °C. Based on the observations of the fracture surface by scanning electron microscope (SEM), the characteristic microstructure of fatigue-induced damage was found for the CF specimens with short dwell times (30 and 120 s). The hardness, elastic modulus and creep deformation near the fracture edges of four typical CF specimens with 30, 120, 600 and 900 s dwell times were measured by nanoindentation. Compared to specimens with post-weld heat treatment (PWHT), lower hardness and creep strength were found for all CF specimens. In addition, significant reductions in hardness, elastic modulus, and creep strength were measured near the fracture edges for the CF specimens with short dwell times compared to the PWHT specimens. Compared to PWHT specimens (0.007), the increased strain rate sensitivities (SRS) of 0.010 to 0.17 were estimated from secondary creep. The increased values of SRS indicate that the room temperature creeps behavior is strongly affected by the decrease in dislocation density after the CF tests.

Curve Fitting for Damage Evolution through Regression Analysis for the Kachanov–Rabotnov Model to the Norton–Bailey Creep Law of SS-316 Material

In a number of circumstances, the Kachanov–Rabotnov isotropic creep damage constitutive model has been utilized to assess the creep deformation of high-temperature components. Secondary creep behavior is usually studied using analytical methods, whereas tertiary creep damage constants are determined by the combination of experiments and numerical optimization. To obtain the tertiary creep damage constants, these methods necessitate extensive computational effort and time to determine the tertiary creep damage constants. In this study, a curve-fitting technique was proposed for applying the Kachanov–Rabotnov model into the built-in Norton–Bailey model in Abaqus. It extrapolates the creep behaviour by fitting the Kachanov–Rabotnov model to the limited creep data obtained from the Omega-Norton–Bailey regression model and then simulates beyond the available data points. Through the Omega creep model, several creep strain rates for SS-316 were calculated using API-579/ASME FFS-1 standards. These are dependent on the type of the material, the flow stress, and the temperature. In the present work, FEA creep assessment was carried out on the SS-316 dog bone specimen, which was used as a material coupon to forecast time-dependent permanent plastic deformation as well as creep behavior at elevated temperatures and under uniform stress. The model was validated with the help of published experimental creep test data, and data optimization for sensitivity study was conducted by applying response surface methodology (RSM) and ANOVA techniques. The results showed that the specimen underwent secondary creep deformation for most of the analysis period. Hence, the method is useful in predicting the complete creep behavior of the material and in generating a creep curve.

Creep Parameters Determination by Omega Model to Norton Bailey Law by Regression Analysis for Austenitic Steel SS-304

In the material’s creep failure analysis, the difficulty of assessing the applied thermo-mechanical boundary conditions makes it critically important. Numerous creep laws have been established over the years to predict the creep deformation, damage evolution and rupture of the materials subjected to creep phenomena. The omega model developed by the American Petroleum Institute and Material Properties Council is one of the most commonly used creep material models for numerical analysis over the years. It is good in defining the fitness of mechanical equipment for service engineering evaluation to ensure the reliable service life of the equipment. The Omega model, however, is not readily accessible and specifically incorporated for creep evaluation in FEA software codes and creep data is always scarce for the complete analysis. Therefore, extrapolation of creep behavior was performed by fitting various types of creep models with a limited amount of creep data and then simulating them, beyond the available data points. In conjunction with the Norton Bailey model, based on API-579/ASME FFS-1 standards, a curve fitting technique was employed called regression analysis. From the MPC project omega model, different creep strain rates were obtained based on material, stress and temperature-dependent data. In addition, as the strain rates increased exponentially with the increase in stresses, regression analysis was used for predicting creep parameters, that can curve fit the data into the embedded Norton Bailey model. The uncertainties in extrapolations and material constants has highlighted to necessitate conservative safety factors for design requirement. In this case study, FEA creep assessment was performed on the material SS-304 dog bone specimen, considered as a material coupon to predict time-dependent plastic deformation along with creep behavior at elevated temperatures and under constant stresses. The results indicated that the specimen underwent secondary creep deformation for most of the period.

Observations of the creep of polar firn

Constant-load creep tests were performed at −10°C at various compressive stresses from 0.05 to 0.75 MPa on specimens taken every 10 m along a firn core extracted at Summit, Greenland in June 2017. The microstructures before and after creep testing were examined using both X-ray microtomography (micro-CT) and optical images from thin sections. An Andrade-like equation was used to describe the primary creep behavior and yielded the time exponent k of 0.17–0.76. The onset of secondary creep occurred at strains of ~0.5–3% but was sometimes not observed at all in shallow firn specimens and at stresses ⩽0.43 MPa even for strain up to 32%. For the 50–80 m firn crept at stresses ⩾0.55 MPa, secondary creep occurred at strains of 2.6 ± 0.28%, and the stress exponent, n, in Glen's law, was found to range from 4.1 to 4.6, similar to those observed for fully dense ice. Micro-CT observations of crept specimens showed that in most cases, the specific surface area, the total porosity and the structure model index decreased, while the structure thickness increased with increasing density. These microstructural characteristics are consistent with the densification of the firn. Optical images from thin sections showed that recrystallization occurred in some specimens that had undergone secondary creep.

Softening of Temperate Ice by Interstitial Water

Ice at depth in ice-stream shear margins is thought to commonly be temperate, with interstitial meltwater that softens ice. Models that include this softening extrapolate results of a single experimental study in which ice effective viscosity decreased by a factor of ∼3 over water contents of ∼0.01–0.8%. Modeling indicates this softening by water localizes strain in shear margins and through shear heating increases meltwater at the bed, enhancing basal slip. To extend data to higher water contents, we shear lab-made ice in confined compression with a large ring-shear device. Ice rings with initial mean grain sizes of 2–4 mm are kept at the pressure-melting temperature and sheared at controlled rates with peak stresses of ∼0.06–0.20 MPa, spanning most of the estimated shear-stress range in West Antarctic shear margins. Final mean grain sizes are 8–13 mm. Water content is measured by inducing a freezing front at the ice-ring edges, tracking its movement inward with thermistors, and fitting the data with solutions of the relevant Stefan problem. Results indicate two creep regimes, below and above a water content of ∼0.6%. Comparison of effective viscosity values in secondary creep with those of tertiary creep from the earlier experimental study indicate that for water contents of 0.2–0.6%, viscosity in secondary creep is about twice as sensitive to water content than for ice sheared to tertiary creep. Above water contents of 0.6%, viscosity values in secondary creep are within 25% of those of tertiary creep, suggesting a stress-limiting mechanism at water contents greater than 0.6% that is insensitive to ice fabric development in tertiary creep. At water contents of ∼0.6–1.7%, effective viscosity is independent of water content, and ice is nearly linear-viscous. Minimization of intercrystalline stress heterogeneity by grain-scale melting and refreezing at rates that approach an upper bound as grain-boundary water films thicken might account for the two regimes.

Rigorous Analysis of Stress-Dependent Landslide Movements with Groundwater Fluctuations Applicable to Disaster Prevention in Monsoon Asia

In this study, novel finite element approaches are proposed for numerical analysis of stress-dependent landslide movement with groundwater fluctuation by rainfall. Two new constitutive parameters that are capable of directly controlling the relationship between the apparent factor of safety and sliding velocity are incorporated into a specific material formulation used in finite element analysis for the first time. For the numerical simulation of the measured time history of the sliding displacement caused by the groundwater fluctuations, such required analytical parameters can also approximately be determined by back analysis. The proposed models are applied to a landslide field experiment on a natural slope caused by rainfall in real time in Futtsu City, Chiba Prefecture of Japan to check its applicability. The predicted and measured time histories along the horizontal direction on the upper, middle, and lower slope are compared. In addition, the deformation pattern, shear strain pattern, and possible failure mechanisms of the natural slope of such a field experiment landslide are discussed in detail based on the analysis results of the finite element method (FEM)-based numerical simulation. Moreover, the creeping landslides and possible landslide sites for further application of the proposed models are briefly discussed in the cases of Nepal and Japan as examples in Asia. It is believed that the proposed newly developed numerical models will help in understanding the secondary creep behavior of landslides triggered by extreme rainfall, and at the same time, long-term management of such landslides will be much easier in monsoon Asia. Finally, it is expected that this study will be extended for simulation of the tertiary creep behavior of landslides induced by rainfall in the near future.

Extended Residual-State Creep Test and Its Application for Landslide Stability Assessment

This paper contains the results of a newly developed residual-state creep test performed to determine the behavior of a selected geomaterial in the context of reactivated landslides. Soil and rock creep is a time-dependent phenomenon in which a deformation occurs under constant stress. Based on the examination results, it was found that the tested clayey material (from Kobe, Japan) shows tertiary creep behavior only under shear stress higher than the residual strength condition and primary and secondary creep behavior under shear stress lower or equal to the residual strength condition. Based on the data, a model for predicting the critical or failure time is introduced. The study traces the development of the limit state based on the contact model corresponding to Blair’s body. The time to occurrence of the conditions necessary for unlimited creep on the surface is estimated. As long-term precipitation and infiltrating water in the area of the landslides are identified as the key phenomena initiating collapse, the work focuses on the prediction of landslides with identified surfaces of potential damage as a result of changes in the saturation state. The procedure outlined is applied to a case study and considerations as to when the necessary safety work should be carried out are presented.

Creep Damage Repair of a Nickel-Based Single Crystal Superalloy Based on Heat Treatment

Taking nickel-based single crystal superalloy DD6 as the research object, different degrees of creep damage were prefabricated by creep interruption tests, and then the creep damage was repaired by the restoration heat treatment system of solid solution heat treatment and two-stage aging heat treatment. The results show that with the creep time increasing, the alloy underwent microstructure evolution including γ′ phase coarsening, N-type rafting and de-rafting. After the restoration heat treatment, the coarse rafted γ′ phase of creep damaged specimens dissolved, precipitated, grew up, and became cubic again. Except for the specimens with creep interruption of 100 h, the γ′ phase can basically achieve the same arrangement as the γ′ phase of the original sample. The comparison of the secondary creep test shows that the steady-state creep stage of the test piece after the restoration heat treatment is relatively increased, and the total creep life can reach the same level as the primary creep life. The high temperature creep properties of the tested alloy are basically recovered, and the restoration heat treatment effect is good.