optical microstructure
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Coatings ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 1564
Author(s):  
Supat Chupradit ◽  
Shameen Ashfaq ◽  
Dmitry Bokov ◽  
Wanich Suksatan ◽  
Abduladheem Turki Jalil ◽  
...  

This study proposes a refractive index sensor for the simultaneous detection of cancer and diabetes based on photonic crystals (PhC). The proposed PhC composed of silicon rods in the air bed arranged in a hexagonal lattice forms the fundamental structure. Two tubes are used to place the cancerous or diabetic samples for measurement. The sensor’s transmission characteristics are simulated and analyzed by solving Maxwell’s electromagnetic equations using the finite-difference time-domain approach for samples being studied. Therefore, diabetes and cancer are detected according to the changes in the refractive index of the samples using the laser source centered at 1550 nm. Considering the findings, the sensor’s geometry changes to adjust the suggested sensitivity and quality factor of structure. According to the results, transmission power ranges between 91 and 100% based on the sample. Moreover, sensitivity ranges from 1294 to 3080 nm/RIU and the maximum Figure of Mertie is nearly FOM = 1550.11 ± 150.11 RIU−1 with the detection in range 31 × 10−6 RIU. In addition, the small area (61.56 μm2) of biosensor results in its appropriateness for different uses in compact photonic integrated circuits. Next, we changed the shape of the dielectric rods and investigated their effects on the sensitivity parameter. The sensitivity and figure of merit after changes in the shape of dielectric rods and nanocavities are at best S = 20,393 nm/RIU and FOM = 9104.017 ± 606.93 RIU−1, receptively. In addition, the resolution detection range is 203.93 × 10−6 RIU.


2021 ◽  
Vol 8 ◽  
Author(s):  
Ateekh Ur Rehman ◽  
Nagumothu Kishore Babu ◽  
Mahesh Kumar Talari ◽  
Yusuf Siraj Usmani ◽  
Hisham Al-Khalefah

In the present study, a rotary friction process was used to join nitinol in a similar welding combination. Macro- and microstructure characteristics of the weld zone were compared with adjacent zones and the base metal. The hardness and tensile properties of the joints were evaluated, and the results were discussed in relation to the weld microstructure. The weld macrostructure revealed a uniform flash around the circumference of the weld. The optical microstructure of the welded sample revealed fine recrystallized grains at the weld interface due to heavy deformation followed by dynamic recrystallization. The phase transformation behavior of the base metal and welded samples was studied by using a differential scanning calorimeter (DSC). The drift in phase transformation temperatures after rotary friction welding may be attributed to fine grain formation at the weld interface. Friction welded samples exhibited improved yield strength and hardness values compared to the base metal due to grain refinement at the weld interface.


2020 ◽  
Vol 1 (1) ◽  
pp. 20-30
Author(s):  
C. Thangamani ◽  
S.Revathi ◽  
P. Matheswaran ◽  
K. Pushpanathan

Ni1-xMnxO (x = 0.0 - 0.05) nanoparticles were successfully prepared by precipitation method at room temperature Prepared samples were characterized by structural, optical, microstructure and magnetic properties. X-ray diffraction analysis confirmed that Mn ions substitution of NiO lattice with FCC structure. The average crystalline size found to decrease from 42 to 34 nm. Optical analysis show increase in band from 4 -3.8 eV by strong quantum confinement effect with blue shift in the absorption spectra range of 325 – 290 nm. FTIR spectra confirmed the formation of Ni-Mn-O.


2020 ◽  
Vol 57 (2) ◽  
pp. 173-188
Author(s):  
Habib Rasouli ◽  
Behzad Fatahi ◽  
Sanjay Nimbalkar

Post-liquefaction response of lightly cemented sands during an earthquake may change and become similar to uncemented sands due to bonding breakage. In the current study, the effect of degree of cementation on liquefaction and post-liquefaction behaviour of lightly cemented sands was studied through a series of cyclic and monotonic triaxial tests. Portland cement with high early strength and Sydney sand were used to reconstitute the lightly cemented specimens with unconfined compression strength ranging from 25 to 220 kPa. A series of multi-stage soil element tests including stress-controlled cyclic loading events with different amplitudes and post-cyclic undrained monotonic shearing tests were carried out on both uncemented and cemented specimens. Furthermore, a series of undrained monotonic shearing tests without cyclic loading history on different types of specimens was conducted to investigate the effect of cyclic loading history on the post-cyclic response of the specimens. The results show that residual excess pore-water pressure is correlated to the cyclic degradation of lightly cemented sands during cyclic loading. In addition, optical microstructure images of the cemented specimens after liquefaction showed that a major proportion of cementation bonds remained unbroken, which resulted in a superior post-liquefaction response with respect to initial stiffness and shear modulus in comparison to the uncemented sand.


POROS ◽  
2018 ◽  
Vol 16 (1) ◽  
Author(s):  
Priyani Budiyarti Budiyarti

AA7075-T6 aluminum alloy is a material that widely used in the aircraft industry because aluminum as a lightweight metal, good machinability, good corrosion resistance and good castability and non-magnetic metals. Aluminum also has high tenacity, is easy to form and is easy to connect. Aluminum has good resistance to corrosion, however aluminum has effect to corrosion if it is on corrosive environment including AA7075-T6 aluminum alloy which used in the aircraft industry. Inhibitor is used to control a corrosion. The aims of these researchs were to investigate the effect of inhibitors on corrosion rates and the rate of fatigue crack corrosion propagation on AA7075-T6 aluminum alloys. This research is used Na2CrO4 inhibitors with variety of concentrations of 0.1%, 0.3%, 0.5% and 0.7% added to 3.5% NaCl solution. Corrosion rate test is used a method of potential dynamic polarization. Corrosion fatigue testing is carried out with constant amplitude at a frequency of 10 Hz and a voltage ratio (R) 0.1. Specimens were used cracked specimen centers (CCT) on orientation in the direction of rolling. The supporting data of the research were the mechanical properties of the material included optical microstructure observation, tensile testing and hardness testing. The results have shown that the optimal concentration of Na2CrO4 inhibitors was achieved at 0.5% which was characterized by a decreasing in corrosion rate and slower corrosion rate of fatigue cracking.


2018 ◽  
Vol 37 (4) ◽  
pp. 333-339
Author(s):  
V. Anil Kumar ◽  
R. K Gupta ◽  
Vinod Kumar ◽  
P. V Venkitakrishnan

AbstractMicrostructure evolution in Co-20Cr-15W-10Ni alloy with hot deformation and subsequent annealing has been studied using hot isothermal compression at different temperatures and strain rates followed by annealing at 1,423 K for 1 h. In the as-deformed condition, optical microstructure reveals deformation bands in specimens deformed at low temperature (1,323 K) and high strain rate (10 s–1). In deformation beyond 1,423 K, very fine recrystallized grains are observed at all the strain rates, which is seen to be fully developed at 1,473 K onwards especially at lower strain rates (0.1 and 0.01 s–1). EBSD maps reveal recrystallized grains and presence of deformation twins. Grain growth is observed at strain rate lower than 0.1 s–1 and temperature more than 1,473 K. After annealing of deformed samples, fully recrystallized grains and annealing twins have been observed. Samples subjected to prior deformation at higher strain rates showed mixed grains with small banding of recrystallized structure, whereas more uniform recrystallized microstructure is observed at slow strain rates. Microhardness decreases with increase in deformation temperature. However, annealed hardness is found to be increasing marginally with decreasing prior deformation temperature (especially for slower strain rates), attributing to relatively uniform and fine microstructure after annealing.


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