On the isothermal sintering behavior and transparency of glass powders

2021 ◽  
Vol 571 ◽  
pp. 121024
Author(s):  
Yingying Zhou ◽  
Jiayan Zhang ◽  
Yide Chen ◽  
Shujiang Liu
1988 ◽  
Vol 3 (1) ◽  
pp. 122-125 ◽  
Author(s):  
Hans Eckart Exner ◽  
Edward A. Giess

The pronounced anisotropy of shrinkage in the axial and the radial direction, observed in earlier studies on the sintering behavior of cordierite-type glass powder, is investigated in detail. It is shown that a planar orientation of the pore/solid interface exists that gives rise to an oriented shrinkage in the radial direction. The results show that the axial-to-diametral shrinkage ratio increases from a value of 0.3 to approximately 0.7 with increasing density, and that particle size and particle shape of the glass powders have little influence on shrinkage anisotropy.


2009 ◽  
Vol 117 (1365) ◽  
pp. 675-679 ◽  
Author(s):  
Dae Soo JUNG ◽  
You Na KO ◽  
Jang Heui YI ◽  
Seung Kwon HONG ◽  
Yun Chan KANG

2011 ◽  
Vol 412 ◽  
pp. 73-77
Author(s):  
Ying He ◽  
Jun Ming Guo ◽  
Zhao Long Huang ◽  
Gui Yang Liu ◽  
Feng Rui Zhai ◽  
...  

The MgO-Al2O3-SiO2 (MAS) glass powders have been synthesized by low-temperature combustion technique using magnesium nitrate, aluminium nitrate, silicic acid as material, urea as fuel. The crystallization process, sintering behavior and dielectric properties were investigated by means of DTA, XRD, TMA and SEM techniques. The results showed that the glass powders could be sintered at lower than 1000°C. The μ-cordierite phase was first crystallized from glass and then transformed into α-cordierite phase during sintering process. The obtained cordierite-based glass-ceramics at 950°C and 1000°C have low dielectric constant (4.00 ~ 4.96 at 1 MHz), low dielectric dissipation factor (≈ 0.003) and high sintering density (which is above 98% of the theoretical density), which are used for electronic packaging.


2018 ◽  
Vol 69 (5) ◽  
pp. 1272-1275 ◽  
Author(s):  
Camelia Tecu ◽  
Aurora Antoniac ◽  
Gultekin Goller ◽  
Mustafa Guven Gok ◽  
Marius Manole ◽  
...  

Bone reconstruction is a complex process which involves an osteoconductive matrix, osteoinductive signaling, osteogenic cells, vascularization and mechanical stability. Lately, to improve the healing of the bone defects and to accelerate the bone fusion and bone augmentation, bioceramic composite materials have been used as bone substitutes in the field of orthopedics and dentistry, as well as in cosmetic surgery. Of all types of bioceramics, the most used is hydroxyapatite, because of its similar properties to those of the human bone and better mechanical properties compared to b-tricalcium phosphate [1]. Currently, the most used raw materials sources for obtaining the hydroxyapatite are: bovine bone, seashells, corals, oyster shell, eggshells and human teeth. There are two common ways to obtain hydroxyapatite: synthetically and naturally. Generally, for the improvement of the mechanical properties and the structural one, hydroxyapatite is subjected to the sintering process. Considering the disadvantages of hydroxyapatite such as poor biodegradation rate, b-TCP has been developed, which has some disadvantages too, such as brittleness. For this reason, the aim of this study is to look into the effect of adding magnesium oxide on the sintering behavior, the structure and the mechanical properties of the hydroxyapatite-tricalcium phosphate composites.


2020 ◽  
Vol 16 (4) ◽  
pp. 578-583
Author(s):  
Muhammad Asif Hussain ◽  
Adnan Maqbool ◽  
Abbas Saeed Hakeem ◽  
Fazal Ahmad Khalid ◽  
Muhammad Asif Rafiq ◽  
...  

Background: The development of new bioimplants with enhanced mechanical and biomedical properties have great impetus for researchers in the field of biomaterials. Metallic materials such as stainless steel 316L (SS316L), applied for bioimplants are compatible to the human osteoblast cells and bear good toughness. However, they suffer by corrosion and their elastic moduli are very high than the application where they need to be used. On the other hand, ceramics such as hydroxyapatite (HAP), is biocompatible as well as bioactive material and helps in bone grafting during the course of bone recovery, it has the inherent brittle nature and low fracture toughness. Therefore, to overcome these issues, a hybrid combination of HAP, SS316L and carbon nanotubes (CNTs) has been synthesized and characterized in the present investigation. Methods: CNTs were acid treated to functionalize their surface and cleaned prior their addition to the composites. The mixing of nano-hydroxyapatite (HAPn), SS316L and CNTs was carried out by nitrogen gas purging followed by the ball milling to insure the homogeneous mixing of the powders. In three compositions, monolithic HAPn, nanocomposites of CNTs reinforced HAPn, and hybrid nanocomposites of CNTs and SS316L reinforced HAPn has been fabricated by spark plasma sintering (SPS) technique. Results: SEM analysis of SPS samples showed enhanced sintering of HAP-CNT nanocomposites, which also showed significant sintering behavior when combined with SS316L. Good densification was achieved in the nanocomposites. No phase change was observed for HAP at relatively higher sintering temperatures (1100°C) of SPS and tricalcium phosphate phase was not detected by XRD analysis. This represents the characteristic advantage with enhanced sintering behavior by SPS technique. Fracture toughness was found to increase with the addition of CNTs and SS316L in HAPn, while hardness initially enhanced with the addition of nonreinforcement (CNTs) in HAPn and then decrease for HAPn-CNT-SS316L hybrid nanocomposites due to presence of SS316L. Conclusion: A homogeneous distribution of CNTs and SPS technique resulted in the improved mechanical properties for HAPn-CNT-SS316L hybrid nanocomposites than other composites and suggested their application as bioimplant materials.


2003 ◽  
Vol 426-432 ◽  
pp. 1897-1902
Author(s):  
S. Gedevanishvili ◽  
S.C. Deevi

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