The Effect of Thermocycling on the Adhesion of Self-etching Adhesives on Dental Enamel and Dentin

2007 ◽  
Vol 8 (2) ◽  
pp. 17-24 ◽  
Author(s):  
Alaa Morsy El Araby ◽  
Yousef F. Talic
Keyword(s):  
Bond Strength ◽  
Null Hypothesis ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Dental Enamel ◽  
Single Step ◽  
The Self ◽  
Repeated Measure ◽  
List Type ◽  
Bond Strengths

Abstract Aim The aim of the present study was to investigate the effectiveness of one total-etch self-priming adhesive and two one-step self-etching adhesive systems on the adhesion of a resin composite to both dentin and enamel. The effect of thermocycling on the adhesion was also investigated. The null hypothesis tested was thermocycling would not affect bond strengths to enamel and dentin treated with self-etching adhesives or a total-etch adhesive. Methods and Materials Two single-step self-etching adhesives [Xeno III (XE3) and Prompt L-Pop (PP)] and one two-step total-etch adhesive system (Prime & Bond NT) (P&B NT) were used in this study. Thirty cariesfree unrestored human third molars were used to make specimens of enamel and dentin. Different adhesives were applied on enamel and dentin surfaces according to the manufacturer's instructions then hybrid composite restorative material was condensed on the surface using a mold. The bonded specimens were stored in distilled water at 37°C for 24 hours before being tested. Half of the bonded specimens were tested for shear bond strength without thermocycling. The other half of the test specimens were thermocycled using a thermocycling apparatus in water baths held at 5°C and 55°C with a dwell time of one minute each for 10,000 cycles prior to shear testing. The mean shear bond strength before and after thermocycling was calculated, and the results were subjected to two-way analysis of variance (ANOVA) and repeated measure design to show the interaction between different materials and different times. Results The results showed shear bond strength on both enamel and dentin of the total-etch adhesive and the self-etching adhesives decreased after the specimens were subjected to thermocycling. Conclusions The null hypothesis tested “thermocycling would not affect bond strengths treated with selfetching adhesives” was rejected. Furthermore, the study revealed the following: The shear bond strength to both enamel and dentin of the total-etch adhesive and the self-etching adhesives decreased after the specimens were subjected to thermocycling. XE3 achieved the highest bond strength to both enamel and dentin (26.994±1.17 and 25.22±1.26, respectively). XE3 showed even better bonding after thermocycling to enamel and dentin than the total-etching system or PP. Although PP bonded to enamel showed lower shear bond strength value than XE3, it has durable bond strength even after thermocycling. Citation El Araby AM, Talic YF. The Effect of Thermocycling on the Adhesion of Self-etching Adhesives on Dental Enamel and Dentin. J Contemp Dent Pract 2007 February;(8)2:017-024.

scholarly journals Shear Bond Strengths and Morphological Evaluation of Filled and Unfilled Adhesive Interfaces to Enamel and Dentine

2012 ◽  
Vol 2012 ◽  
pp. 1-9 ◽  
Author(s):  
Vajihesadat Mortazavi ◽  
Mohammadhosein Fathi ◽  
Ebrahim Ataei ◽  
Niloufar Khodaeian ◽  
Navid Askari
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Testing Machine ◽  
The Other ◽  
Adhesive Systems ◽  
Morphological Evaluation ◽  
Bond Strengths ◽  
Post Hoc ◽  
One Way Anova

In this laboratory study shear bond strengths of three filled and one unfilled adhesive systems to enamel and dentine were compared. Forty-eight extracted intact noncarious human mandibular molars were randomly assigned to two groups of 24 one for bonding to enamel and the other for bonding to dentine. Buccal and lingual surfaces of each tooth were randomly assigned for application of each one of filled (Prime & Bond NT (PBNT), Optibond Solo Plus (OBSP), and Clearfil SE Bond (CSEB)) and unfilled (Single Bond (SB)) adhesive systems (n=12). A universal resin composite was placed into the translucent plastic cylinders (3 mm in diameter and 2 mm in length) and seated against the enamel and dentine surfaces and polymerized for 40 seconds. Shear bond strength was determined using a universal testing machine, and the results were statistically analyzed using two-way ANOVA, one-way ANOVA,t-test, and Tukey HSD post hoc test with a 5% level of significance.There were no statistically significant differences in bond strength between the adhesive systems in enamel, but CSEB and SB exhibited significantly higher and lower bond strength to dentine, respectively, than the other tested adhesive systems while there were no statistically significant differences between PBNT and OBSP.

Comparison of the Effect of Hydrogel and a Solution of Sodium Ascorbate on Dentincomposite Bond Strength After Bleaching

2008 ◽  
Vol 9 (2) ◽  
pp. 105-112 ◽  
Author(s):  
Soodabeh Kimyai ◽  
Hadi Valizadeh
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Sodium Ascorbate ◽  
Carbamide Peroxide ◽  
Treatment Groups ◽  
Bleaching Procedure ◽  
Bond Strengths ◽  
Composite Shear ◽  
Group 1

Abstract Aim The aim of this study was to compare the effects of solution and different sodium ascorbate hydrogels on dentin-resin composite shear bond strength subsequent to a bleaching procedure with 10% carbamide peroxide. Methods and Materials Sixty buccal dentin surfaces obtained from intact human third molars were randomly divided into five groups (n=12). Dentin surfaces received different treatments: (1) no treatment; (2) bleaching (10% carbamide peroxide gel); (3) bleaching + 10% sodium ascorbate solution; (4) bleaching + 10% sodium ascorbate hydrogel, and (5) bleaching + 20% sodium ascorbate hydrogel. Dentin surfaces were bonded with Single Bond™ and restored with a composite (Z100). The samples were tested for shear bond strengths. Data was analyzed using analysis of variance (ANOVA) and Tukey tests. Results Significantly higher bond strengths were observed subsequent to treatment with hydrogel and solution forms of sodium ascorbate (p<0.05). No significant differences were demonstrated between different forms of sodium ascorbate preparations. In addition, no significant differences were observed among groups with antioxidant treatment (Groups 3, 4, and 5) and Group 1 (no treatment). Conclusion Reduced bond strength to bleached dentin can be amended by the use of sodium ascorbate as an antioxidant. Clinical Significance Both hydrogel and solution forms of sodium ascorbate can significantly improve the reduced bond strength of resin composite to dentin subsequent to a bleaching procedure with 10% carbamide peroxide. Citation Kimyai S, Valizadeh H. Comparison of the Effect of Hydrogel and a Solution of Sodium Ascorbate on Dentin-composite Bond Strength After Bleaching. J Contemp Dent Pract 2008 February;(9)2:105-112.

scholarly journals The Durability of Zirconia/Resin Composite Shear Bond Strength using Different Functional Monomer of Universal Adhesives

2021 ◽  
Author(s):  
Awiruth Klaisiri ◽  
Nantawan Krajangta ◽  
Niyom Thamrongananskul
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Functional Monomers ◽  
Composite Interface ◽  
Before And After ◽  
Universal Adhesives ◽  
Bond Strengths ◽  
Composite Shear ◽  
One Way Anova

Abstract Objective This study examined the effectiveness of different functional monomers in universal adhesives on zirconia/resin composite bond strength both before and after thermocycling. Four universal adhesives (G-premio bond universal, GPU; Clearfil Tri-S bond universal, CTB; Optibond Universal, OBU; Tetric N-bond universal; TNU), one adhesive (single bond 2; SB2), and one ceramic primer (Clearfil ceramic primer plus, CCP) were used in this study. Materials and Methods Zirconia discs were prepared and embedded in acrylic. Specimens were polished and sandblasted with alumina. The specimens were randomly divided into two groups (24 hours and the thermocycled), and each group was divided into six subgroups (n = 10), according to zirconia surfaces treatments: no Tx, CCP + SB2, GPU, CTB, OBU, TNU. An Ultradent mold was located on top of the treated zirconia surface. The resin composite was filled into the mold and then light-cured. A universal testing device was used to determine the shear bond strength. Statistical Analysis The data were statistically analyzed using one-way ANOVA and Tukey's test. Results After water storage for 24 hours, the shear bond strengths were GPU > CCP + SB2 = CTB = OBU = TNU > no Tx (p < 0.05). After thermocycling, the shear bond strengths were CCP + SB2 = GPU = CTB = TNU > OBU > no Tx (p < 0.05). Conclusion The universal adhesives containing 10-MDP exhibited the best performance in the shear bond strength of the zirconia/resin composite interface both before and after thermocycling.

Comparative Analysis of the Shear Bond Strength of Flowable Self-Adhering Resin-Composites Adhesive to Dentine with a Conventional Adhesive

2021 ◽  
Vol 7 (2) ◽  
Author(s):  
Asiri AA ◽  
◽  
Khan R ◽  
Alzahrani SS ◽  
Haider S ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Adhesive Bonding ◽  
Resin Composite ◽  
Testing Machine ◽  
The Self ◽  
Flowable Composite ◽  
Modes Of Failure ◽  
Group I ◽  
Group Ii

This study aimed to measure and compare the Shear Bond Strength (SBS) of a self-adhering flowable resin composite to dentin with a conventional flowable composite, and evaluate the various modes of failure. Thirty (n=30) human premolar teeth were randomly allocated to two groups (Group I: Vertise Flow; Group II: Filtek Ultimate) of 15 specimens each, and SBS was measured for specimens from each group by applying shear load using a Universal Testing Machine (UTM). Modes of failure were observed with an optical microscope. An independent samples T test was performed to test the Levene’s assumption of homogeneity of variance across both groups, with the critical value set at 0.05. The results revealed, that the self-adhering flowable composite (Group I: VertiseTM Flow) resulted in lower shear bond strength as compared with the conventional flowable resin composite (Group II: Filtek Ultimate). Moreover, group I predominantly exhibited non-cohesive failure which reflects a poor bonding to dentin. On the other hand, Group II showed mixed failure for most of the samples, which demonstrate strong adhesive bonding. Therefore, it could be concluded that the self-adhering flowable resin composite (Group I) results in lower SBS to dentin as compare with conventional flowable composite.

Micro-Shear Bond Strength of Different Adhesives to Human Dental Enamel

2011 ◽  
Vol 35 (3) ◽  
pp. 301-304 ◽  
Author(s):  
MP Nagayassu ◽  
LK Shintome ◽  
VE Arana-Chavez ◽  
M Fava
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Dental Enamel ◽  
Adhesive System ◽  
Shear Testing ◽  
Tukey Test ◽  
Significant Difference ◽  
Acid Etch ◽  
Inner Diameter

The aim of this study was to evaluate the micro-shear bond strength of 5 adhesive systems to enamel, one single-bottle acid-etch adhesive (O), two self-etching primers (P) and two all-in-one self-etching adhesives(S). Method: Sixty premolar enamel surfaces (buccal or lingual) were ground flat with 400- and 600-grit SiC papers and randomly divided into 5 groups (n=12), according to the adhesive system: SB2 - Single Bond 2 (O); CSE - Clearfil SE Bond (P); ADS - AdheSE (P); PLP - Adper Prompt L-Pop (S); XE3 - Xeno III (S). Tygon tubing (inner diameter of 0.8mm) restricted the bonding area to obtain the resin composite(Z250) cylinders. After storage in distilled water at 37° C for 24h and thermocycling, micro-shear testing was performed (crosshead speed of 0.5mm/min). Data were submitted to one-way ANOVA and Tukey test(a=5%). Samples were also subjected to stereomicroscopic and SEM evaluations after micro-shear testing. Mean bond strength values (MPa±SD) and the results of Tukey test were: SB2: 36.36(±3.34)a; ADS:33.03(±7.83)a; XE3: 32.76(±5.61)a; CSE: 30.61(±6.68)a; PLP: 22.17(±6.05)b. Groups with the same letter were not statistically different. It can be concluded that no significant difference was there between SB2,ADS, XE3 and CSE, in spite of different etching patterns of these adhesives. Only PLP presented statistically lower bond strengths compared with others.

Shear-Bond Strength of a New Self-Adhering Flowable Restorative Material to Dentin of Primary Molars

2013 ◽  
Vol 38 (2) ◽  
pp. 149-154 ◽  
Author(s):  
E Pacifici ◽  
M Chazine ◽  
A Vichi ◽  
S Grandini ◽  
C Goracci ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Primary Molars ◽  
Restorative Material ◽  
Chi Square ◽  
Etch And Rinse ◽  
Bond Strengths ◽  
Vertise Flow ◽  
Wallis Anova

Objective: The aim of this study was to evaluate the shear bond strength to dentin of primary molars of a new self-adhering flowable resin composite with two ionomer-based cements and one flowable resin composite in combination with two different adhesive systems. Study design: Fifty primary molars were grinded on the occlusal surface to obtain flat dentin substrate and randomly divided into 5 groups (n=10): OFL:Phosphoric Acid/Optibond FL/Premise Flow; OAO:Optibond All-In-One/Premise Flowable; II:Polyacrylic Acid/Fuji II; IX:Polyacrylic Acid/Fuji IX; V:Vertise Flow. Cylinders (3mm diameter – 5mm height) of restorative material were built-up in three increments over the dentin surfaces. A shear load was applied until failure. Bond strength values were statistically analysed with Kruskall-Wallis ANOVA followed by Dunn's test (P&lt;.05). Differences in failure mode distribution were assessed with Chi-square (P&lt;.05). Results: OFL and OAO recorded significantly higher bond strengths than the other groups. Adhesive failures were evident in all groups except OFL and OAO, in which also cohesive failures in dentin were observed. Conclusions: Vertise Flow established on primary dentin bond strengths values similar to those of glass ionomer cements routinely used for restorations of primary teeth. The combination of flowable resin with etch-and-rinse or all-in-one adhesives obtained higher bond strength values, thus involving a more complex handling.

scholarly journals The effects of application time of a self-etching primer and debonding methods on bracket bond strength

2011 ◽  
Vol 82 (1) ◽  
pp. 131-136 ◽  
Author(s):  
Brandon C. Parrish ◽  
Thomas R. Katona ◽  
Serkis C. Isikbay ◽  
Kelton T. Stewart ◽  
Katherine S. Kula
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
The Self ◽  
Maxillary Incisor ◽  
Application Time ◽  
Adhesive Remnant Index ◽  
Significant Difference ◽  
Bond Strengths ◽  
Variance Testing ◽  
Lift Off

Abstract Objective: To test the manufacturer's recommendation for the application rubbing time of a self-etching primer (Transbond Plus, 3M Unitek) and to compare the resulting bond strength of a resin composite (Transbond XT, 3M Unitek) in the traditional laboratory tension on all four wings with a simulation of the clinical single-wing lift-off debonding instrument (LODI; 3M Unitek). Materials and Methods: Flattened stainless-steel maxillary incisor orthodontic brackets (Victory Series, 3M Unitek) were bonded to 108 flattened bovine incisors. The enamel was rubbed with the self-etching primer for 0, 5 (the manufacturer's recommendation), and 10 seconds during a 10-second application. Traditional four-wing and LODI simulated debonding forces and the adhesive remnant index (ARI) were recorded. Results: One-way analysis of variance testing among rubbing times and debonding methods indicated a significant difference in strength with 0 and 5 seconds of rubbing and between traditional and LODI simulated tension. The bond strengths were higher in the ARI  =  1 subset compared to the ARI  =  3–5 subsets. Conclusions: The manufacturer's recommendation for primer rubbing time produced the highest bond strength. Less force is required for debonding when tension is applied to one wing (LODI simulation) vs on all four wings.

scholarly journals Comparative Analysis of the Shear Bond Strength of Flowable Self-Adhering Resin-Composites Adhesive to Dentin with a Conventional Adhesive

Coatings ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 273
Author(s):  
Abdulmajeed Ali Asiri ◽  
Rawaiz Khan ◽  
Sultan Saeed Alzahrani ◽  
Sajjad Haider ◽  
Salah Ud-Din Khan ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Adhesive System ◽  
The Self ◽  
Single Bond ◽  
Flowable Composite ◽  
Modes Of Failure ◽  
Group I ◽  
Group Ii

This study aimed to measure and compare the shear bond strength (SBS) of a self-adhering flowable resin composite to dentin with a conventional flowable composite, and evaluate the various modes of failure. Thirty human premolar teeth (n = 30) were randomly allocated to two groups (Group I: Vertise™ Flow; Group II: Filtek Ultimate + Single Bond Universal) of 15 specimens each, and SBS was measured for specimens from each group by applying a shear load using a universal testing machine (UTM). Modes of failure were observed with an optical microscope. An independent-samples T-test was performed to test Levene’s assumption of homogeneity of variance across both groups, with the critical value set at 0.05. The results revealed, that the self-adhering flowable composite (Group I: Vertise™ Flow) resulted in a lower shear bond strength compared with the conventional adhesive system composite (Group II: Filtek Ultimate + Single Bond Universal). Moreover, group I predominantly exhibited non-cohesive failure, which reflects poor bonding to dentin. On the other hand, Group II showed mixed failure for most of the samples, which demonstrated strong adhesive bonding. Therefore, it could be concluded that the self-adhering flowable resin composite (Group I) results in lower SBS to dentin compared with a conventional adhesive system.

scholarly journals To Evaluate Shear Bond Strength of Resin Composite to Theracal Lc, Biodentine, and Resin–Modified Glass Ionomer Cement and Mode of Fracture: An In Vitro Study

2020 ◽  
Vol 8 (02) ◽  
pp. 49-54
Author(s):  
Salil Mehra ◽  
Ashu K. Gupta ◽  
Bhanu Pratap Singh ◽  
Mandeep Kaur ◽  
Ashwath Kumar
Keyword(s):  
Statistical Analysis ◽  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Glass Ionomer Cement ◽  
Bonding Agent ◽  
Glass Ionomer ◽  
Universal Adhesive ◽  
Resin Modified Glass Ionomer ◽  
Ionomer Cement

Abstract Introduction The aim of the current study was to evaluate shear bond strength of resin composite bonded to Theracal LC, Biodentine, and resin-modified glass ionomer cement (RMGIC) using universal adhesive and mode of fracture. Materials and Methods A total of 50 caries-free maxillary and mandibular molars extracted were taken; occlusal cavities were prepared, mounted in acrylic blocks, and divided into five groups based on the liner used. Group 1: Biodentine liner placed into the cavity and bonding agent and resin composite applied after 12 minutes. Group 2: Biodentine liner placed into the cavity and bonding agent and resin composite applied after 14 days. Group 3: RMGIC liner placed into the cavity and bonding agent and resin composite applied immediately. Group 4: RMGIC liner placed into the cavity and bonding agent and resin composite applied after 7 days. Group 5: Theracal LC liner placed into the cavity and bonding agent and resin composite applied immediately. Each sample was bonded to resin composite using universal adhesive. Shear bond strength analysis was performed at a cross-head speed of 0.1 mm/min. Statistical Analysis  Statistical analysis was performed with one-way analysis of variance and posthoc Bonferroni test using SPSS version 22.0. Results and Conclusion Biodentine liner when bonded immediately to resin composite showed minimum shear bond strength. RMGIC when bonded to resin composite after 7 days showed maximum shear bond strength. Mode of fracture was predominantly cohesive in groups having Biodentine and Theracal LC as liner.

scholarly journals The Effect of Different Disinfecting Agents on Bond Strength of Resin Composites

2014 ◽  
Vol 2014 ◽  
pp. 1-7 ◽  
Author(s):  
Ahmed Mohammed Hassan ◽  
Ahmed Ali Goda ◽  
Kusai Baroudi
Keyword(s):  
Bond Strength ◽  
Sodium Hypochlorite ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Testing Machine ◽  
Control Group ◽  
Posterior Teeth ◽  
Surface Pretreatment ◽  
Dentin Surface ◽  
Post Hoc

Objective. The aim of this study was to evaluate the effect of different disinfectant agents on bond strength of two types of resin composite materials.Methods. A total of 80 sound posterior teeth were used. They were divided into four groups(n=20)according to the dentin surface pretreatment (no treatment, chlorhexidine gluconate 2%, sodium hypochlorite 4%, and EDTA 19%). Each group was divided into two subgroups according to the type of adhesive (prime and bond 2.1 and Adper easy one). Each subgroup was further divided into two subgroups according to the type of resin composite (TPH spectrum and Tetric EvoCeram). Shear bond strength between dentin and resin composite was measured using Universal Testing Machine. Data collected were statistically analyzed byt-test and one-way ANOVA followed by Tukey’spost hoctest.Results. It was found that dentin treated with EDTA recorded the highest shear bond strength values followed by sodium hypochlorite and then chlorhexidine groups while the control group showed the lowest shear bond strength.Conclusions. The surface treatment of dentin before bonding application has a great effect on shear bond strength between resin composite and dentin surface.

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