Evaluation of the Effect of Cold Plasma Treatment on the Microshear Bond Strength of Composite Resin Restorations to Dentin using Different Adhesive Systems and the Effect of Thermocycling

Introduction: Currently, non-thermal plasma is used to modify the enamel and dentin surfaces to improve the bonding surface to dental composite resins. Non-thermal plasma creates a hydrophilic surface, decreases the contact angle, and improves the bonding quality. The present study aimed to evaluate the microshear bond strength (µSBS) of composite resins to dentin using different adhesive systems. Materials and Methods: Bovine incisor teeth were randomly assigned to three groups of G-Premio, Clearfil SE Bond, and Adper Single Bond adhesive groups after preparation. Each group was divided into two subgroups in terms of argon plasma surface preparation, and each subgroup was divided into two groups in terms of thermocycling (n=12). The microshear bond strength of the samples was determined using a universal testing machine. Three-way ANOVA was used to analyze the effect of the adhesive, plasma preparation, and thermocycling. Post hoc Tukey tests were used for two-by-two comparisons of µSBS. Statistical significance was set at P <0.05. Results: The results of the µSBS test showed that the application of plasma resulted in a significant increase in the mean µSBS in the G-Premio group, with no significant increase in the Clearfil SE bond and Adper Single groups. The effect of thermocycling after plasma application was significant only in the Adper Single group. Conclusion: The application of plasma might increase the bond strength of composite resins to dentin. However, further studies are necessary.

Hydrofluoric acid concentration and etching time on bond strength to lithium disilicate glass-ceramic

The objective of this study to evaluate the effect of different HF concentrations and etching times on the microshear bond strength (μSBS) of LD to resin cement. Forty LD sections (8x8 mm) of 3-mm thickness were randomly distributed (n=10) in accordance with the HF concentration (5 or 10%) and surface etching time (20 or 60 sec). The specimens were silanized and received an air-thinned layer of a light-curable adhesive. Six translucent tubes (0.8-mm diameter and 1-mm height) were positioned over each LD section, filled with resin cement and light-cured. After 24 h of storage, the tubes were carefully removed and the specimens were submitted to the μSBS test. The results submitted to a two-way analysis of variance and Sidak post hoc test (α=.05). Representative HF-etched specimens and one non-etched LD specimen were observed under a field-emission scanning electron microscope. The interaction between the HF concentrations and etching times was not significant (p=0.075). No significant differences were observed regarding HF concentrations and etching times (p=0.06 and p=0.059, respectively). Surfaces of specimens etched with 10% HF for 60 sec were found with grooves and microcracks. The μSBS of LD to resin cement was not significantly influenced by different HF concentrations and etching times; however, the LD surface morphology was found considerably modified.

Comparison of Bond Strength in the Different Class of Resin Cements to Cast and CAD/CAM Co-Cr Alloys

Objectives. Despite the widespread use of resin cements in cementing dental restorations, their bond strength to CAD/CAM base metal alloys is not widely studied. This study aimed to evaluate the microshear bond strength (μSBS) between cobalt-chrome (Co-Cr) alloys fabricated using casting or CAD/CAM methods with three types of resin cements. Materials and Methods. Fifty Co-Cr blocks were prepared with CAD/CAM or casting technique. Specimens were divided using primer or not and bonded to three types of resin cements: Panavia F2, RelyX Unicem, and Duo-Link. The differences between the mean μSBS values were analyzed using the two-way ANOVA test and Tukey analysis (α = 0.05). The mode of failure was evaluated using a stereomicroscope. In addition, the specimens were examined by scanning electron microscopy (SEM) based on two received signals: backscattered electrons (SEB) and secondary electrons (SEs). One intact alloy specimen in each group was analyzed by energy-dispersive X-ray spectroscopy (EDX). Results. Most of the specimens in the no-primer group were prematurely debonded. Statistical analyses showed that the interaction between the alloy substrate and cement type was significant ( p = 0.001 ). The bond strength of Panavia F2 was significantly higher than Duo-Link in the CAD/CAM group ( p = 0.001 ). SEM evaluation confirmed the difference in grain structures, while EDX showed no remarkable difference in the chemical composition of the alloy substrates. Conclusion. Alloy fabrication technique may influence the bond strength of resin cements. In the CAD/CAM group, cement containing MDP molecules exhibited higher strength than the etch-and-rinse one.

Effect of Simultaneous Sintering of Bioglass to a Zirconia Core on Properties and Bond Strength

This study aimed to assess bioglass sintering to a zirconia core on surface properties and bonding strength to resin cement. Zirconia specimens were divided into four groups: G I: sintered; G II: bioglass modified zirconia (a bioglass slurry was sintered with zirconia at 1550 °C); G III: sandblasted using 50 μm Al2O3 particles; and G IV: Z-prime plus application. Surface morphology and chemical analysis were studied using a scanning electron microscope and energy-dispersive spectroscopy. Surface roughness was evaluated using a profilometer. Surface hardness was measured using an indentation tester. For the microshear bond strength test, resin cement cylinders were bonded to a zirconia surface. Half of the specimens were tested after 24 h; the other half were thermocycled (5–55 °C) for 1000 cycles. A shearing load was applied at a crosshead speed of 0.5 mm/min on a universal testing machine. Data were analyzed with ANOVA using SPSS software at (p < 0.05). Results: tThe mean surface roughness of G II was significantly higher than G I and G III. The microhardness of G II was significantly lower than all groups. For bond strength, there was no significant difference between groups II, III, and IV after thermocycling. Conclusions: Bioactive glass can increase the bond strength of zirconia to resin cement, and is comparable to sandblasting and Z-prime bonding agents.

Effect of Exposure Times of Sodium Hypochlorite before Acid Etching on the Microshear Bond Strength to Fluorotic Enamel

Purpose: To evaluate the effects of different treatment time of 5.25% Sodium hypochlorite (NaOCl) on the microshear bond strength (μSBS), attenuated total reflection Fourier transform infrared (ATR-FTIR) and etching pattern in mild and moderate fluorotic enamel. Study design: Forty-eight fluorotic molars were divided into two groups: mild and moderate fluorotic enamel which were classified by a Thylstrup and Fejerskov index (TFI). Based on the application time (0s, 60s, 120s, 180s) of 5.25% NaOCl, each group was sectioned into four parts. Then the etched enamel was bonded with resin and tested to acquire μSBS. The statistical method was two-way ANOVA and Least Significant Difference (LSD) test at α = 0.05. Besides, fracture modes were observed under a stereo microscope. SEM was used to evaluated the enamel-etching pattern and organic content on the fluorotic enamel surface were investigated by ATR-FTIR. Results: Duration of 5.25% NaOCl at 60s or 120s significantly increased the μSBS of fluorotic enamel compared to 0s (p&lt;0.05). Fracture modes indicated that dominating failures were set in the bonding interface but whose proportion decreased when 5.25% NaOCl was applied. The enamel-etching pattern in 180s was deepest under SEM. Spectra of enamel samples manifested an obvious and gradual removal of its organic phase after duration of NaOCl increased. Conclusion: The maximal μSBS is acquired by using 5.25% NaOCl at 60s for mild fluorotic enamel but 120s for the moderate. The prolonged application time of 5.25% NaOCl prior to phosphoric acid etching improves enamel-etching pattern. Treatment of 5.25% NaOCl decreases proteins on the fluorotic enamel surface.

Remineralization potential and mechanical evaluation of a bioactive glass containing composite (An ex vivo study)

AIM: The aim of this study was to compare the remineralization ability, ion release, microshear bond strength and wear resistance of a claimed bioactive restorative material (ACTIVA BioACTIVE Restorative, Pulpdent Corporation, Watertown, USA) with the conventional resin composite (​Filtek Z350 XT, 3M ESPE Elipar, Germany). MATERIALS AND METHODS: The remineralization ability was evaluated after 28 days using Energy Dispersive X-Ray (EDX) analysis. Ion release was investigated at three-time intervals: 1, 14 and 28 days. Calcium and phosphate ions release were determined by using ion chromatography system. Microshear bond strength was assessed using Universal Testing Machine. A wear test was conducted using a dual axis chewing simulator. RESULTS: ACTIVA™ was found to induce remineralization to the demineralized dentin. Results revealed that ACTIVA™ released Ca2+ and PO4-3 ions, whilst Filtek Z350 XT did not. Concerning microshear bond strength ACTIVA™ without adhesive application showed unacceptable failure. Regarding wear resistance there was no statistically significant difference between them. CONCLUSION: ACTIVA™ bioactive restorative material seems promising bioactive restorative materials. Clinical trials are recommended to compare clinical performance of ACTIVA™ with the other restorative materials.

Effect of Die Spacer Thickness on the Microshear Bond Strength of CAD/CAM Lithium Disilicate Veneers

Aim. The aim of this study was to compare the microshear bond strength of ceramic veneers with digital die spacer settings at 20, 40, and 100 µm. Materials and Methods. Eighteen milled lithium disilicate microdiscs (IPS e.max CAD, Ivoclar Vivadent) were divided into three groups (n = 6) according to their digital die spacer settings: group A = 20 µm, group B = 40 µm, and group C = 100 µm. Six randomly selected sound maxillary premolars received three microdiscs each. Each microdisc was 1 mm in diameter and 1 mm in height. The buccal surfaces of the premolars were prepared with a 0.5 mm depth in enamel. After cementation, the specimens were thermocycled for 2,500 cycles between 5 and 55°C. Microshear bond strength testing was performed using a universal testing machine until bonding failure. Failure modes were evaluated using a stereomicroscope. Statistical analyses included one-way ANOVA, Tukey’s post hoc test, and chi-square test with a 5% alpha error and 80% study power. Results. The mean microshear bond strength values were calculated in MPa for group A = 31.91 ± 12.41, group B = 29.58 ± 5.03, and group C = 13.85 ± 4.12. One-way ANOVA ( p ≤ 0.05 ) showed a statistically significant difference in microshear bond strength among the three groups. Tukey’s post hoc test showed significant differences between groups A and C ( p = 0.004 ) and between groups B and C ( p = 0.011 ). The failure modes were presented as cohesive, adhesive, and mixed failures. Chi-square test indicated that the failure mode distribution was not significantly different among the three groups ( p = 0.970 ). Conclusion. Higher digital die spacer settings decrease the microshear bond strength of CAD/CAM lithium disilicate veneers.

Bond strength of resin composite to enamel submitted to at-home desensitizer and bleaching agents

Aim: This study evaluated the effect of a desensitizer agent (DES) during bleaching with 10% carbamide peroxide (CP) on enamel microshear bond strength (μSBS). Methods: Sixty bovine incisors were obtained and randomly distributed into groups (n=15): (C) Control: no desensitizing or bleaching, (DES) desensitizing gel application, (CP) bleaching with 10% CP and (CP/DES) bleaching with 10% CP combined with DES. Bleaching was performed for 6 h/day for 14 consecutive days. DES was applied for 8 h only on the 7th and 14th days of therapy. Specimens were stored in artificial saliva among the CP or DES applications and submitted to μSBS testing at three postrestoration times (n=5): 24 h, 7 days, and 14 days after bleaching using a universal testing machine. Failure modes were observed under a stereomicroscope. Data were analyzed by two-way ANOVA and Tukey’s test (α=5%). Results: Immediately after bleaching (24 h), CP promoted lower μSBS than the C and DES groups (p<0.05) but with no differences from the CP/DES. μSBS increased in the DES, CP, and CP/DES groups (p<0.05) when bonding was performed for 7 or 14 days elapsed from bleaching. CP/DES exhibited the highest μSBS among the groups 14 days after bleaching (p<0.05). Cohesive failure in enamel was predominant in the CP groups, while adhesive failure was mostly observed for the other groups. Conclusion: The use of a desensitizer during at-home bleaching maintained the enamel immediate bond strength, and its application favored bonding when the restoration was delayed for 14 days.